2,4,6-三甲基环三硅氧烷合成路线 (共 5 条)
反应条件
diethyl ether; d-N,a-dimethylphenethylamine Erhitzen des Reaktionsgemisches auf 300-350grad;
参考文献
Brewer
Journal of the American Chemical Society, 1948 , vol. 70, p. 3962
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Gmelin Handbook: Si: MVol.C, 99, page 271 - 274
反应条件
hydrogenchloride in toluene T=20°C; 4 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Kopylov, V. M.; Agashkov, S. P.; Sunkovich, G. V.; Prikhod'ko, P. L.; Ezerets, M. A.; Glukhova, M. A.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 9.2 p. 2100 - 2106,1873 - 1878
反应条件
hydrogenchloride in toluene T=20°C; 4 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Kopylov, V. M.; Agashkov, S. P.; Sunkovich, G. V.; Prikhod'ko, P. L.; Ezerets, M. A.; Glukhova, M. A.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 9.2 p. 2100 - 2106,1873 - 1878
反应条件
Erhitzen des Reaktionsgemisches auf 300-350grad;
参考文献
Brewer
Journal of the American Chemical Society, 1948 , vol. 70, p. 3962
反应条件
in not given ((CH3)HSiO)3 and traces of aq. acid for a few days;; distn.;;
参考文献
Brewer
Journal of the American Chemical Society, 1948 , vol. 70, p. 3962
Full Text View citing articles Show Details
Gmelin Handbook: Si: MVol.C, 99, page 271 - 274