4-甲基-1,2,4-三吖啉-3,5-二酮合成路线 (共 19 条)
反应条件
silica gel; periodic acid; sodium nitrite in dichloromethane T=20°C; 1.5 h;
参考文献
Zolfigol, Mohammad Ali; Madrakian, Elaheh; Ghaemi, Ezat; Mallakpour, Shadpour
Synlett, 2002 , # 10 p. 1633 - 1636
反应条件
1,1,2,2-tetramethylethylene; anhydrous dichloroethane in chloroform-d1 T=29°C; Decomposition; cycloreversion; KineticsThermodynamic data; Further Variations:SolventsTemperatures;
参考文献
Journal of Organic Chemistry, , vol. 65, # 10 p. 2863 - 2869
反应条件
1,1,2,2-tetramethylethylene; anhydrous dichloroethane in chloroform-d1 T=29°C; Decomposition; cycloreversion; Kinetics;
参考文献
Journal of Organic Chemistry, , vol. 65, # 10 p. 2863 - 2869
反应条件
in chloroform-d1 T=-20.1 - 19.9°C; Equilibrium constant;
参考文献
Journal of Physical Organic Chemistry, , vol. 10, # 6 p. 456 - 460
反应条件
in dichloromethane -78 deg C to 10 deg C;
参考文献
Askani, Rainer; Schneider, Wilfried
Chemische Berichte, 1983 , vol. 116, # 6 p. 2355 - 2365
反应条件
in tetrahydrofuran Ambient temperature1) 0 deg C, 2) CH3Br, room temperature, 6 h; prototype reaction, oth. alcohols, oth. phosphine; Product distribution;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 57, # 9 p. 2675 - 2676
反应条件
in tetrachloroethane, 1,1,2,2- T=20°C; Diels-Alder reaction; 1 h;
参考文献
European Journal of Organic Chemistry, , # 19 p. 3811 - 3817
反应条件
in tetrachloroethane, 1,1,2,2- 4 h; UV-irradiation;
参考文献
European Journal of Organic Chemistry, , # 19 p. 3811 - 3817
反应条件
in tetrachloroethane, 1,1,2,2- 0.5 h; UV-irradiation;
参考文献
European Journal of Organic Chemistry, , # 19 p. 3811 - 3817
反应条件
in tetrachloroethane, 1,1,2,2- 2 h; UV-irradiation;
参考文献
European Journal of Organic Chemistry, , # 19 p. 3811 - 3817