4-甲基-1,2,4-三吖啉-3,5-二酮合成路线 （共 19 条）
反应条件
in dichloromethane 0.0833333 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 42, # 19 p. 5273 - 5280
反应条件
in tetrahydrofuran Ambient temperature1) 0 deg C, 2) CH3I, room temperature, 6 h; prototype reaction, oth. alcohols, oth. phosphine; Product distribution;
参考文献
Oshikawa, Tatsuo; Yamashita, Mitsuji
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 9 p. 2675 - 2676
反应条件
T=-263.2°C; Irradiationfurther 4-R-1,2,4-triazoline-3,5-diones; Product distributionRate constant;
参考文献
Risi, Florence; Pizzala, Louis; Carles, Micheline; Verlaque, Patrick; Aycard, Jean-Pierre
Journal of Organic Chemistry, 1996 , vol. 61, # 2 p. 666 - 670
反应条件
water in tetrahydrofuran; dichloromethane T=0°C; Condensation;
参考文献
Organic Letters, , vol. 2, # 10 p. 1383 - 1385
反应条件
in dichloromethane 0.0833333 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 42, # 19 p. 5273 - 5280
反应条件
in dichloromethane
T=0 - 5°C;
参考文献
Hall, J. Herbert; Krishnan, Ganapathy
Journal of Organic Chemistry, 1984 , vol. 49, # 13 p. 2498 - 2500
反应条件
hydrogen; palladium on activated charcoal
1) CH2Cl2, 2) EE, 45 psi; Yield given. Multistep reaction;
参考文献
Nelsen, Stephen F.; Petillo, Peter A.; Chang, Hao; Frigo, Timothy B.; Dougherty, Dennis A.; Kaftory, Menahem
Journal of Organic Chemistry, 1991 , vol. 56, # 18 p. 613 - 618
反应条件
in tetrahydrofuran
Ambient temperature1) 0 deg C, 2) CH3Br, room temperature, 6 h; prototype reaction, oth. alcohols, oth. phosphine; Product distribution;
参考文献
Oshikawa, Tatsuo; Yamashita, Mitsuji
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 9 p. 2675 - 2676
反应条件
in tetrahydrofuran
Ambient temperature1) 0 deg C, 2) CH3I, room temperature, 6 h; prototype reaction, oth. alcohols, oth. phosphine; Product distribution;
参考文献
Oshikawa, Tatsuo; Yamashita, Mitsuji
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 9 p. 2675 - 2676
