1,1,1,3-四氯丁烷合成路线 （共 26 条）
反应条件
tetrachloromethane; sulfuryl dichloride; dibenzoyl peroxide
参考文献
Brown; Ash
Journal of the American Chemical Society, 1955 , vol. 77, p. 4019,4023
反应条件
hexacarbonyl chromium
T=120°C; 0.5 h; nucleophilic additives; Product distribution;
参考文献
Grigor'ev, N. A.; Tumanskaya, A. L.; Freidlina, R. Kh.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 7 p. 1215 - 1218
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 7 p. 1515 - 1518
反应条件
tetrachloromethane
heating to 60°C during 32 h;
参考文献
Vyazankin, N. S.; Brevnova, T. N.; Razuvaev, G. A.
Zhurnal Obshchei Khimii, 1967 , vol. 37, p. 187 - 189
Zhurnal Obshchei Khimii, 1967 , vol. 37, p. 204 - 207
反应条件
tetrachloromethane
byproducts: CHCl3; 100°C in closed tube for 16 h;
参考文献
Vyazankin, N. S.; Brevnova, T. N.; Razuvaev, G. A.
Zhurnal Obshchei Khimii, 1967 , vol. 37, p. 187 - 189
Zhurnal Obshchei Khimii, 1967 , vol. 37, p. 204 - 207
Full Text Show Details
Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.2.4.7, page 73 - 76
参考文献
Kharasch; Jensen; Urry
Journal of the American Chemical Society, 1947 , vol. 69, p. 1104
反应条件
(i) Co2(CO)8, (ii) aq. NH3; Multistep reaction;
参考文献
Susuki,T.; Tsuji,J.
Journal of Organic Chemistry, 1970 , vol. 35, p. 2982 - 2986
反应条件
di-tert-butyl peroxide; triphenylphosphine
T=140°C; 1 h; chain termination in the telomerization of title compound; Product distributionMechanism;
参考文献
Freidlina, R. Kh.; Tumanskaya, A. L.; Vitt, S. V.; Grigor'ev, N. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, # 12 p. 2641 - 2643
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , # 12 p. 2844 - 2847
参考文献
Brown; Ash
Journal of the American Chemical Society, 1955 , vol. 77, p. 4019,4023
反应条件
di-tert-butyl peroxide
T=140°C; 1 h; chain termination in the telomerization of title compound; Product distributionMechanism;
参考文献
Freidlina, R. Kh.; Tumanskaya, A. L.; Vitt, S. V.; Grigor'ev, N. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, # 12 p. 2641 - 2643
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , # 12 p. 2844 - 2847
反应条件
W(CO)6
T=140°C; 1 h; chain termination in the telomerization of title compound; Product distributionMechanism;
参考文献
Freidlina, R. Kh.; Tumanskaya, A. L.; Vitt, S. V.; Grigor'ev, N. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, # 12 p. 2641 - 2643
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , # 12 p. 2844 - 2847
