4-氯-2-丁炔-1-醇合成路线 (共 37 条)
反应条件
copper(l) iodide; potassium carbonate; sodium iodide in N,N-dimethyl-formamide 5 h; Ambient temperature;
参考文献
Lapitskaya; Vasiljeva; Pivnitsky
Synthesis, 1993 , # 1 p. 65 - 66
反应条件
(i) Mg, THF, (ii) /BRN= 1098382/, CuCl, THF; Multistep reaction;
参考文献
Ege,S.N. et al.
Journal of the American Chemical Society, 1961 , vol. 83, p. 3080 - 3085
参考文献
Organic Letters, , vol. 6, # 10 p. 1673 - 1675
参考文献
Colonge; Poilane
Bulletin de la Societe Chimique de France, 1955 , p. 502
反应条件
potassium carbonate in acetone 8 h; Heating;
参考文献
Majumdar, Krishna C.; Jana, Gour H.; Das, Udayan
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 8 p. 1229 - 1231
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Lehrich, Friedhelm; Hopf, Henning; Grunenberg, Joerg
European Journal of Organic Chemistry, 2011 , # 14 p. 2705 - 2718
参考文献
Bailey; Pfeifer
Journal of Organic Chemistry, 1955 , vol. 20, p. 1337,1340
反应条件
(i) Et3N, (ii) aq. NaOH; Multistep reaction;
参考文献
Brel',V.K. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1978 , vol. 48, p. 2791,2531
反应条件
in diethyl ether
T=5°C;
参考文献
Gelin,R. et al.
Bulletin de la Societe Chimique de France, 1971 , p. 4146 - 4152
反应条件
potassium hydroxide in water
1.) 4 h, r. t., 2.) 2 h, heating;
参考文献
Rudorf, W.-D.; Janietz, D.
Journal fuer Praktische Chemie (Leipzig), 1987 , vol. 329, # 1 p. 55 - 61