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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
132855-24-4
合成路线
（共 10 条）
75-97-8
频哪酮
+
7570-98-1
→
反应条件
529-36-2
1-奈硫酚
+
6721-67-1
3,3-二甲基-1-苯基-2-丁酮
+
132855-24-4
+
108-98-5
硫酚
反应条件
potassium tert-butylate in dimethyl sulfoxide T=25°C; 5 h; Irradiation; Further byproducts given;
参考文献
Cheng, Carlos; Stock, Leon M.
Journal of Organic Chemistry, 1991 , vol. 56, # 7 p. 2436 - 2443
75-97-8
频哪酮
+
607-53-4
→
反应条件
91-20-3
萘
+
529-36-2
1-奈硫酚
+
604-53-5
1,1'-联萘
+
132855-24-4
反应条件
potassium tert-butylate in N,N-dimethyl-formamide T=25°C; 19 h; Irradiation;
参考文献
Cheng, Carlos; Stock, Leon M.
Journal of Organic Chemistry, 1991 , vol. 56, # 7 p. 2436 - 2443
90-14-2
1-碘萘
+
351531-29-8
→
反应条件
132855-24-4
反应条件
in ammonia T=-33°C; 0.583333 h; Irradiation;
参考文献
Bunnett, Joseph F.; Mitchel, Eric; Galli, Carlo
Tetrahedron, 1985 , vol. 41, # 19 p. 4119 - 4132
90-11-9
1-溴代萘
+
351531-29-8
→
反应条件
91-20-3
萘
+
132855-24-4
反应条件
potassium tert-butylate in dimethyl sulfoxide T=25°C; Irradiation; Kinetics;
参考文献
Annunziata, Alfonso; Galli, Carlo; Marinelli, Manuela; Pau, Tullia
European Journal of Organic Chemistry, 2001 , # 7 p. 1323 - 1329
75-97-8
频哪酮
+
90-11-9
1-溴代萘
→
反应条件
132855-24-4
反应条件
potassium tert-butylate in ammonia T=-33°C; Irradiationrelative reactivity in competition with bromobenzene; Rate constantMechanism;
参考文献
Galli, Carlo
Gazzetta Chimica Italiana, 1988 , vol. 118, # 5 p. 365 - 368
75-97-8
频哪酮
+
90-11-9
1-溴代萘
→
反应条件
91-20-3
萘
+
132855-24-4
反应条件
potassium tert-butylate; iron(II) chloride 1.) DMSO, RT, 20 min, 2.) DMSO, RT, 20 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Galli, Carlo; Gentili, Patrizia
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 6 p. 1135 - 1140
75-97-8
频哪酮
+
90-14-2
1-碘萘
→
反应条件
91-20-3
萘
+
132855-24-4
反应条件
potassium tert-butylate; iron(II) chloride 1.) DMSO, RT, 20 min, 2.) DMSO, RT, 20 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Galli, Carlo; Gentili, Patrizia
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 6 p. 1135 - 1140
64723-95-1
+
90-11-9
1-溴代萘
+
29800-93-9
→
反应条件
25944-75-6
二乙基1-萘基膦酸酯
+
132855-24-4
反应条件
in ammonia T=-33°C; Irradiationcompetitive reaction, at known concentrations; relative rate constants, half life; Product distribution;
参考文献
Bunnett, Joseph F.; Mitchel, Eric; Galli, Carlo
Tetrahedron, 1985 , vol. 41, # 19 p. 4119 - 4132
64723-95-1
+
90-14-2
1-碘萘
+
29800-93-9
→
反应条件
25944-75-6
二乙基1-萘基膦酸酯
+
132855-24-4
反应条件
in ammonia T=-33°C; Irradiationcompetitive reaction, at known concentrations; relative rate constants, half life; Product distribution;
参考文献
Bunnett, Joseph F.; Mitchel, Eric; Galli, Carlo
Tetrahedron, 1985 , vol. 41, # 19 p. 4119 - 4132
64723-95-1
+
29800-93-9
+
90-13-1
α-氯代萘
→
反应条件
25944-75-6
二乙基1-萘基膦酸酯
+
132855-24-4
反应条件
in ammonia T=-33°C; Irradiationcompetitive reaction, at known concentrations; relative rate constants, half life; Product distribution;
参考文献
Bunnett, Joseph F.; Mitchel, Eric; Galli, Carlo
Tetrahedron, 1985 , vol. 41, # 19 p. 4119 - 4132
