2-(1,3-二噻吩)磷酸二甲酯合成路线 （共 5 条）
反应条件
sodium iodide in acetonitrile 2 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 1 p. 157 - 168
反应条件
in acetonitrile 1 h;
参考文献
Journal of the American Chemical Society, , vol. 115, # 9 p. 3752 - 3759
反应条件
n-butyllithium 1) THF, -78 deg C, 0.5h, 2) -78 deg C, 1h, -> 20 deg C, 12h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Moore, Adrian J.; Bryce, Martin R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 1 p. 157 - 168
反应条件
n-butyllithium 1) THF, -78 deg C, 0.5h, 2) -78 deg C, 1h, -> 20 deg C, 12h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Moore, Adrian J.; Bryce, Martin R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 1 p. 157 - 168
反应条件
1: dimethyl (1,3-dithiol-2-yl)phosphonate With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 0.166667 h;
2: N-(4,5-dihexyl-1,3-dithiol-2-ylidene)piperidinium hexafluorophosphate in tetrahydrofuran; hexane
T=20°C; 0.75 h;
3: With acetic acid in tetrahydrofuran; hexane
2 h;
参考文献
Andersson, Asbjorn Sune; Kilsa, Kristine; Hassenkam, Tue; Gisselbrecht, Jean-Paul; Boudon, Corinne; Gross, Maurice; Nielsen, Mogens Brondsted; Diederich, Francois
Chemistry - A European Journal, 2006 , vol. 12, # 33 p. 8451 - 8459
