2,2-二氟-1-苯基-1,3-丁二酮合成路线 (共 4 条)
反应条件
N-fluorobislt;(trifluoromethyl)sulfonylgt;imide in dichloromethane T=22°C; 24 h;
参考文献
Stavber, Gaj; Stavber, Stojan
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 16 p. 2838 - 2846
反应条件
water; 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate); gold(I) chloride in acetonitrile T=85°C;
参考文献
Schuler, Marie; Silva, Franck; Bobbio, Carla; Tessier, Arnaud; Gouverneur, Veronique
Angewandte Chemie - International Edition, 2008 , vol. 47, # 41 p. 7927 - 7930
反应条件
1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate); triethylamine in acetonitrile T=-10°C; 0.5 h;
参考文献
Peng, Weimin; Shreeve, Jean'ne M.
Journal of Organic Chemistry, 2005 , vol. 70, # 14 p. 5760 - 5763
反应条件
1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate); triethylamine in acetonitrile T=-10°C; 0.5 h;
参考文献
Peng, Weimin; Shreeve, Jean'ne M.
Journal of Organic Chemistry, 2005 , vol. 70, # 14 p. 5760 - 5763