2-乙氧基-4,5,6,7-四氢-3H-氮杂卓合成路线 （共 16 条）
反应条件
boron trifluoride-diethyl ether complex in dichloromethane
参考文献
Sterling Drug Inc.
Patent: US3963748 A1, 1976 ;
参考文献
Menezes, Royce; Smith, Michael B.
Synthetic Communications, 1988 , vol. 18, # 4 p. 1625 - 1636
反应条件
crystalline zeolite-containing catalist in water T=325 - 370°C; Beckmann Rearrangement;
参考文献
Sumitomo Chemical Company, Limited
Patent: US6344557 B1, 2002 ;
Location in patent: Page column 7-8 ;
反应条件
pyridine; chloroform; benzenesulfonyl chloride und anschliessend mit Aethanol;
参考文献
Knoll and Co.
Patent: DE531403 , 1929 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 18, p. 3052
反应条件
hydrogen azide; benzene und anschliessend mit Aethanol und Phosphorylchlorid;
参考文献
Knoll and Co.
Patent: DE488447 , 1926 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 18, p. 3048
参考文献
Knoll and Co.
Patent: DE532969 , 1929 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 18, p. 3050
反应条件
T=180 - 250°C; unter Stickstoff;
参考文献
Benson; Cairns
Journal of the American Chemical Society, 1948 , vol. 70, p. 2115,2116
Org.Synth.Coll.Vol., 1963 , vol. IV, p. 588
反应条件
1: hydrazine hydrate 2: water; acetic acid; NaNO2 View Scheme
参考文献
Stolle
Chemische Berichte, 1930 , vol. 63, p. 1032,1033
反应条件
1: 78 percent / HCl / diethyl ether / 0.17 h 2: 90 percent / H2O / 24 h / Ambient temperature View Scheme
参考文献
Menezes, Royce; Smith, Michael B.
Synthetic Communications, 1988 , vol. 18, # 4 p. 1625 - 1636
参考文献
Stolle
Chemische Berichte, 1930 , vol. 63, p. 1032,1033
