7-乙酰氧基双环(2.2.1)-2,5-庚二烯合成路线 （共 5 条）
反应条件
1.) flash vacuum thermolysis, 510 deg C, 2.) cocondensation with argon; var.: thermolysis at 600 deg C; Multistep reaction;
参考文献
McMahon, Robert J.; Abelt, Christopher J.; Chapman, Orville L.; Johnson, Jeffery W.; Kreil, Curits L.; et al.
Journal of the American Chemical Society, 1987 , vol. 109, # 8 p. 2456 - 2469
反应条件
T=745°C; var.: temperature; Product distribution;
参考文献
McMahon, Robert J.; Abelt, Christopher J.; Chapman, Orville L.; Johnson, Jeffery W.; Kreil, Curits L.; et al.
Journal of the American Chemical Society, 1987 , vol. 109, # 8 p. 2456 - 2469
反应条件
T=700°C; Yields of byproduct given;
参考文献
Hoffmann, Reinhard W.; Loof, Ingo H.; Wentrup, Curt
Liebigs Annalen der Chemie, 1980 , # 8 p. 1198 - 1206
反应条件
in hexane; acetone 5 h; IrradiationInert atmosphere;
参考文献
Sletten, Ellen May; Bertozzi, Carolyn Ruth
Patent: US2013/244267 A1, 2013 ;
Location in patent: Paragraph 0302 ;
反应条件
1.) flash vacuum thermolysis, 510 deg C, 2.) cocondensation with argon; var.: thermolysis at 600 deg C; Multistep reaction;
参考文献
McMahon, Robert J.; Abelt, Christopher J.; Chapman, Orville L.; Johnson, Jeffery W.; Kreil, Curits L.; et al.
Journal of the American Chemical Society, 1987 , vol. 109, # 8 p. 2456 - 2469
