In(OSO2CF3)3 in acetonitrile T=20°C; Acetylation;

1: 2-methyl-3-(4-methylbenzoyloxy)-2-((4-(trifluoromethyl)benzoyloxy)methyl)propyl 3,5-bis(trifluoromethyl)benzoate With N,N,N',N',N'',N''-hexamethylphosphoric triamide; samarium diiodide in tetrahydrofuran RefluxInert atmosphere; 2: acetic anhydride With 4-(N,N-dimethlyamino)pyridine; triethylamine

sulfuric acid T=130 - 140°C; unter Druck;

sulfuric acid

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