in dichloromethane byproducts: AgI; Sonication; under N2 or Ar atm.; I2 sublimed onto the solid Ag(P4)2Al(OC(CF3)3)4 at 77 K, then CH2Cl2 condensed onto mixt.; placed in dry ice/2-propanol bath; then stored at -80 °C with heavy shaking; soln. filtered; volatiles removed at 0 °C;
参考文献
Krossing; Raabe
Angewandte Chemie - International Edition, 2001 , vol. 40, # 23 p. 4406 - 4409
