反应条件
in dichloromethane under N2, molar ratio Re-compd.:BI3 = 1:1.2, dropwise addn. of BJ3 in CH2Cl2 to a soln. of Re-compd. in CH2Cl2 at -20°C, stirred for 1.5 h at -20°C; evapn. of solvent, addn. of pentane, frozen in liquid N2, warmed to -78°C, removal of pentane soln., washed (pentane, -80°C), dried, extn. (pentane), evapn., cooled to -78°C, recrystn., dried (vac., -10°C, 3h); elem. anal.;
参考文献
Filippou, Alexander Constantin; Fischer, Ernst Otto; Alt, Helmut Guido
Journal of Organometallic Chemistry, 1987 , vol. 330, p. 325 - 336
