N,N-二甲基-2-萘甲酰胺合成路线 （共 20 条）
反应条件
tert.-butylhydroperoxide; Cu2(4,4’-biphenyldicarboxylate)2(4,4’-bipyridine) T=100°C;
参考文献
Phan, Nam T.S.; Nguyen, Tung T.; Vu, Phuong H. L.
ChemCatChem, 2013 , vol. 5, # 10 p. 3068 - 3077
反应条件
hydrogenchloride Yield given;
参考文献
Boche, Gernot; Bosold, Ferdinand; Niessner, Manfred
Tetrahedron Letters, 1982 , vol. 23, # 32 p. 3255 - 3256
反应条件
1: 1.) lithium diisopropylamide / 2.) 5 h 2: 2n HCl View Scheme
参考文献
Boche, Gernot; Bosold, Ferdinand; Niessner, Manfred
Tetrahedron Letters, 1982 , vol. 23, # 32 p. 3255 - 3256
反应条件
2: 1.) lithium diisopropylamide / 2.) 5 h 3: 2n HCl View Scheme
参考文献
Boche, Gernot; Bosold, Ferdinand; Niessner, Manfred
Tetrahedron Letters, 1982 , vol. 23, # 32 p. 3255 - 3256
反应条件
tin(IV) chloride T=100 - 105°C; 3 h; other reagent - AlCl3; Product distribution;
参考文献
Isakova, A. P.; Naumov, Yu. A.; Nikeryasova, S. V.; Fomichev, A. A.; Murugova, L. A.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, # 3 p. 558 - 561
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 3 p. 639 - 642
反应条件
LDBMOA in tetrahydrofuran; hexane T=0°C; 0.5 h;
参考文献
Kim, Yu Ri; An, Duk Keun
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 12 p. 4194 - 4196
反应条件
1: With disodium hydrogenphosphate in acetonitrile T=20°C; Methylation; 18 h; 2: With sodium hydrogencarbonate Hydrolysis; 18 h;
参考文献
Keck, Gary E; McLaws, Mark D; Wager, Travis T
Tetrahedron, 2000 , vol. 56, # 51 p. 9875 - 9883
反应条件
1: With diisobutylaluminium hydride in tetrahydrofuran; hexane T=-78°C; 1.5 h; Inert atmosphere; 2: With ammonia; iodine in tetrahydrofuran; hexane; water T=0 - 20°C; Inert atmosphere;
参考文献
Suzuki, Yusuke; Yoshino, Takumi; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2011 , vol. 67, # 21 p. 3809 - 3814
反应条件
methanol-d1; water-d2; tert.-butyl lithium
1.) THF, pentane, -45 deg C, 30 min, 2.) 2 h, room t.,; Yield given. Multistep reaction;
参考文献
Meyers, A.I.; Lutomski, Kathryn A.; Laucher, Dominique
Tetrahedron, 1988 , vol. 44, # 11 p. 3107 - 3118
反应条件
methanol-d1; water-d2
1.) THF, pentane, -45 deg C, 30 min, 2.) 2 h, room t.,; Yield given. Multistep reaction;
参考文献
Meyers, A.I.; Lutomski, Kathryn A.; Laucher, Dominique
Tetrahedron, 1988 , vol. 44, # 11 p. 3107 - 3118
