3-(3-噻吩)-2-丙酸甲酯合成路线 （共 4 条）
反应条件
sodium hydride in tetrahydrofuran T=20°C; 12 h;
参考文献
THE REGENTS OF THE UNIVERSITY OF CALIFORNIA; HE, Biao; MANN, Michael; JABLONS, David, M.
Patent: WO2013/13190 A1, 2013 ;
Location in patent: Paragraph 00216 ;
反应条件
3-methoxy-2-hydroxybenzaldehydeiminato(thiosemicarbazone)(triphenylphosphane)palladium(II); sodium carbonate in N,N-dimethyl-formamide T=140°C; Mizoroki-Heck reaction; 24 h; Inert atmosphere;
参考文献
Xie, Guanlei; Chellan, Prinessa; Mao, Jincheng; Chibale, Kelly; Smith, Gregory S.
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 10 p. 1641 - 1647
反应条件
in dichloromethane Wittig reaction;
参考文献
Martins, Andrew; Lautens, Mark
Journal of Organic Chemistry, 2008 , vol. 73, # 22 p. 8705 - 8710
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Martins, Andrew; Lautens, Mark
Journal of Organic Chemistry, 2008 , vol. 73, # 22 p. 8705 - 8710
