1,3-苯二酚单苯甲酸酯合成路线 (共 26 条)
参考文献
Justus Liebigs Annalen der Chemie, , vol. 301, p. 104
参考文献
Chemische Berichte, , vol. 53, p. 1629
反应条件
1: 76 percent / PPh3; diisopropyl azodicarboxylate / tetrahydrofuran 2: 99 percent / aq. NaOH / methanol View Scheme
参考文献
Boxhall, Jonathan Y.; Page, Philip C. Bulman; Chan, Yohan; Hayman, Colin M.; Heaney, Harry; McGrath, Matthew J.
Synlett, 2003 , # 7 p. 997 - 1001
反应条件
N,N-dimethyl-formamide; silver(l) oxide Behandeln des erhaltenen Reaktionsprodukts mit aethanol. KOH;
参考文献
Freudenberg; Alonso de Lama
Justus Liebigs Annalen der Chemie, 1958 , vol. 612, p. 78,88
反应条件
1: anhydrous chloroform; bromine 2: aqueous NaOH 3: K2CO3; water View Scheme
参考文献
Hodgson; Dyson
Journal of the Chemical Society, 1935 , p. 946
参考文献
Fischer,E.
Chemische Berichte, 1920 , vol. 53, p. 1629
反应条件
potassium carbonate; sodium iodide in acetone 2 h; Inert atmosphere; SolventReagent/catalyst;
参考文献
Prasad, Kapa; Xu, David D.; Tempkin, Orin; Villhauer, Edwin B.; Repic, Oljan
Organic Process Research and Development, 2003 , vol. 7, # 5 p. 743 - 749
参考文献
Fischer,E.
Chemische Berichte, 1920 , vol. 53, p. 1629
反应条件
nitric acid; acetic acid man verseift das entstandene Gemisch mit Natronlauge;
参考文献
Kauffmann; Kugel
Chemische Berichte, 1911 , vol. 44, p. 755
反应条件
1.1: sodium carbonate / di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium / toluene / 100 °C / Inert atmosphere 2.1: diethylzinc / 1,2-dichloro-ethane / 0 - 20 °C 3.1: sodium hydroxide; water / tetrahydrofuran; methanol / 1.5 h / 20 °C 3.2: pH ~ 1 View Scheme
参考文献
PFIZER INC.; ASPNES, Gary Erik; DIDIUK, Mary Theresa; GUZMAN-PEREZ, Angel; MAGUIRE, Robert John
Patent: WO2011/158149 A1, 2011 ;
WO 2011/158149 A1