3-氯-2-氧代三苯基磷酸亚苯酯合成路线 （共 12 条）
反应条件
sodium carbonate in methanol T=20°C; 0.75 h;
参考文献
Taillier, Catherine; Hameury, Thomas; Bellosta, Veronique; Cossy, Janine
Tetrahedron, 2007 , vol. 63, # 21 p. 4472 - 4490
反应条件
1: in tetrahydrofuran 4 h; Heating; 2: With sodium carbonate in methanol T=20°C; 0.5 h;
参考文献
Lanaspeze, Sebastien; Neier, Reinhard
Monatshefte fur Chemie, 2005 , vol. 136, # 4 p. 597 - 607
反应条件
1: 73 percent / tetrahydrofuran / 4 h / Heating 2: 89 percent / Na2CO3 / methanol; H2O / 0.5 h / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 61, # 28 p. 6871 - 6878
反应条件
in methanol Heating;
参考文献
Baker,B.R.; Jordaan,H.
Journal of Medicinal Chemistry, 1965 , vol. 8, p. 35 - 41
参考文献
Baker,B.R.; Jordaan,H.
Journal of Medicinal Chemistry, 1965 , vol. 8, p. 35 - 41
参考文献
Baker; Ho
Journal of pharmaceutical sciences, 1967 , vol. 56, # 1 p. 28 - 32
反应条件
sodium hydride in N,N-dimethyl-formamide 6 h; Ambient temperature;
参考文献
Caballero, Esther; Guilhot, Fabien; Lopez, Jose Luis; Medarde, Manuel; Sahagun, Heidi; Tome, Fernando
Tetrahedron Letters, 1996 , vol. 37, # 38 p. 6951 - 6954
参考文献
Henichart; Houssin; Bernier
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 5 p. 1531 - 1533
反应条件
sodium hydride 1. DMF, 30 min, room temperature 2. 4 h, 70-80 deg C; Yield given. Multistep reaction;
参考文献
Flitsch, Wilhelm; Hohenhorst, Manfred
Liebigs Annalen der Chemie, 1990 , # 4 p. 397 - 399
反应条件
sodium ethanolate; potassium iodide in tetrahydrofuran
T=70°C; 12 h;
参考文献
Lin, Yuh-Lin; Kuo, Hsien-Shou; Wang, Yi-Wen; Huang, Sheng-Tung
Tetrahedron, 2003 , vol. 59, # 8 p. 1277 - 1281
