136918-14-4合成路线 （共 708 条）
反应条件
1: alcohol; hydrazine hydrate 2: PCl5 3: nitrobenzene / 180 °C View Scheme
参考文献
Drew; Hatt
Journal of the Chemical Society, 1937 , p. 16,25
反应条件
1: With bromine; sodium hydroxide in water T=-5°C; 0.0333333 h; Reflux; 2: With hydrogenchloride in water pH=4 - 5;
参考文献
Yin, Ruijuan; Zhang, Meng; Hao, Cui; Wang, Wei; Qiu, Peiju; Wan, Shengbiao; Zhang, Lijuan; Jiang, Tao
Chemical Communications, 2013 , vol. 49, # 76 p. 8516 - 8518
参考文献
Tscherniac
Chemische Berichte, 1903 , vol. 36, p. 218
反应条件
potassium hydroxide; 1-n-butyl-3-methylimidazolium tetrafluoroborate T=50°C; 5 h;
参考文献
Le, Zhang-Gao; Chen, Zhen-Chu; Hu, Yi; Zheng, Qin-Guo
Synthesis, 2004 , # 2 p. 208 - 212
反应条件
PhP(C6H4-p-(CH2)2C6F13)2; diethylazodicarboxylate in tetrahydrofuran
参考文献
Dandapani, Sivaraman; Curran, Dennis P.
Tetrahedron, 2002 , vol. 58, # 20 p. 3855 - 3864
反应条件
cesium fluoride in acetonitrile 48 h; Heating;
参考文献
Hayat, Safdar; Atta-Ur-Rahman; Iqbal Choudhary; Khan, Khalid Mohammed; Schumann, Wilhelm; Bayer, Ernst
Tetrahedron, 2001 , vol. 57, # 50 p. 9951 - 9957
反应条件
1: With [bis(acetoxy)iodo]benzene T=145°C; 3 h; Microwave irradiation; 2: With hydrazine hydrate in water; acetonitrile
参考文献
Kantak, Abhishek A.; Potavathri, Shathaverdhan; Barham, Rose A.; Romano, Kaitlyn M.; Deboef, Brenton
Journal of the American Chemical Society, 2011 , vol. 133, # 49 p. 19960 - 19965
反应条件
caesium carbonate in N,N-dimethyl-formamide T=70°C; 2 h;
参考文献
Escudero, Mercedes Isasmendi; Kremenchuzky, Lautaro D.; Perillo, Isabel A.; Cerecetto, Hugo; Blanco, Maria M.
Synthesis, 2011 , # 4 art. no. M06310SS, p. 571 - 576
反应条件
di-isopropyl azodicarboxylate; triphenylphosphine in tetrahydrofuran 3 h; Product distribution / selectivity;
参考文献
DRAXIS Specialty Pharmaceuticals Inc.
Patent: US2008/102028 A1, 2008 ;
Location in patent: Page/Page column 9; 10-11 ;
反应条件
diethylazodicarboxylate in tetrahydrofuran 2 h;
参考文献
Grynkiewicz, Grzegorz
Polish Journal of Chemistry, 1982 , vol. 56, # 1 p. 149 - 152
