136918-14-4合成路线 (共 708 条)
反应条件
diethylazodicarboxylate in tetrahydrofuran 2 h;
参考文献
Grynkiewicz, Grzegorz
Polish Journal of Chemistry, 1982 , vol. 56, # 1 p. 149 - 152
反应条件
chloro-trimethyl-silane T=40°C; 5 h;
参考文献
Xue, Cuihua; Luo, Fen-Tair
Journal of the Chinese Chemical Society, 2004 , vol. 51, # 2 p. 359 - 362
反应条件
sulfuric acid; iodine T=75 - 80°C; 24 h;
参考文献
Journal of Organic Chemistry, , vol. 61, # 9 p. 3034 - 3040
反应条件
1: With sulfuric acid; iodine T=80 - 85°C; 40 h; 2: With potassium hydroxide 12 h; Heating;
参考文献
Jiang, Jinyue; Kaafarani, Bilal R.; Neckers, Douglas C.
Journal of Organic Chemistry, 2006 , vol. 71, # 5 p. 2155 - 2158
反应条件
water; 1,4-diaza-bicyclo[2.2.2]octane T=30°C; other catalysts; Rate constantMechanism;
参考文献
Aslam, Hanif M.; Burden, Alan G.; Chapman, Norman B.; Shorter, John; Charton, Marvin
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 500 - 508
反应条件
in water; acetonitrile T=35°C; effect of solvent ratio; Rate constant;
参考文献
Khan, M. Niyaz
Journal of Physical Organic Chemistry, 1999 , vol. 12, # 3 p. 187 - 193
反应条件
ammonium hydroxide 1.5 h; Ambient temperatureother imides if aromatic acids; other time; Product distributionMechanism;
参考文献
Arkhipova, i. A.; Gabdrakipov, V. Z.; Shalabaeva, I. D.; Zhubanov, B. A.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 3.2 p. 535 - 540
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 3 p. 621 - 628
反应条件
titanium tetrachloride; zinc in tetrahydrofuran T=0°C; 12 h;
参考文献
Kise, Naoki; Kawano, Yusuke; Sakurai, Toshihiko
Journal of Organic Chemistry, 2013 , vol. 78, # 24 p. 12453 - 12459
反应条件
1: phthalimide; 4-hydroxy-5-hexenenitrile With triphenylphosphine in tetrahydrofuran T=0°C; 0.166667 h; 2: di-isopropyl azodicarboxylate in tetrahydrofuran T=0 - 20°C; 3.33 h;
参考文献
NORTHWESTERN UNIVERSITY
Patent: WO2007/35964 A2, 2007 ;
Location in patent: Page/Page column 9; 16 ;
反应条件
water; sodium hydroxide T=130°C; 13 h;
参考文献
SHODHANA LABORATORIES LIMITED
Patent: WO2009/128088 A2, 2009 ;
Location in patent: Page/Page column 11; 12 ;