136918-14-4合成路线 (共 708 条)
反应条件
1: alcohol; hydrazine hydrate 2: PCl5 View Scheme
参考文献
Drew; Hatt
Journal of the Chemical Society, 1937 , p. 16,25
反应条件
1.1: sodium hydroxide; bromine / water / 0.03 h / -5 °C / |Reflux 1.2: pH 4 - 5 2.1: N,N-dimethyl-formamide / 0 - 20 °C View Scheme
参考文献
Chemical Communications, , vol. 49, # 76 p. 8516 - 8518
反应条件
sodium hydroxide; Methyl methyltrioctylammonium sulfate in toluene T=95°C; 4 h; different bases, other temperatures; Product distribution;
参考文献
Journal of applied chemistry of the USSR, , vol. 60, # 1 pt 2 p. 220 - 222
反应条件
potassium carbonate beim Erwaermen des Reaktionsprodukts mit Hydrazin-hydrat und Aethanol;
参考文献
Halpern et al.
Journal of the American Pharmaceutical Association (1912-1977), 1951 , vol. 40, p. 6
反应条件
toluene-4-sulfonic acid in N,N-dimethyl-formamide T=100°C; 10 h; Product distribution / selectivity;
参考文献
UNIVERSITY COLLEGE CORK - NATIONAL UNIVERSITY OF IRELAND, CORK
Patent: WO2009/34169 A1, 2009 ;
Location in patent: Page/Page column 22-24 ;
反应条件
toluene-4-sulfonic acid in N,N-dimethyl-formamide T=100°C; 10 h; Product distribution / selectivity;
参考文献
UNIVERSITY COLLEGE CORK - NATIONAL UNIVERSITY OF IRELAND, CORK
Patent: WO2009/34169 A1, 2009 ;
Location in patent: Page/Page column 24 ;
反应条件
hexaammonium heptamolybdate tetrahydrate T=120°C; 0.166667 h; Microwave irradiation;
参考文献
Seyyedhamzeh, Mozhdeh; Ganji, Nasim; Shaabani, Ahmad
Journal of Porphyrins and Phthalocyanines, 2012 , vol. 16, # 10 p. 1110 - 1113
反应条件
ammonium molibdate; copper(II) sulfate heptahydrate; urea 0.05 h; HeatingMicrowave irradiation;
参考文献
Kumar, Vishal; Sharma, Upendra; Verma, Praveen K.; Kumar, Neeraj; Singh, Bikram
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 5 p. 870 - 878
反应条件
potassium carbonate; N,N-dimethyl-formamide anschl. mit wss. NaOH;
参考文献
Int. Minerals and Chem. Corp.
Patent: US2757198 , 1953 ;
反应条件
sodium hydroxide; sodium hypochlorite; water
参考文献
Mohr
Journal fuer Praktische Chemie (Leipzig), 1909 , vol. <2> 80, p. 10,14, 18, 24
Full Text Show Details
Hoechster Farbw.
Patent: DE127138 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 6, p. 156