136918-14-4合成路线 （共 708 条）
反应条件
1: 56 percent / H2SO4; HNO3 / 0.67 h / 40 - 50 °C 2: 65 percent / SnCl2; HCl / H2O / 2 h / 50 °C View Scheme
参考文献
Warrener, Ronald N.; Liu, Ligong; Russell, Richard A.
Tetrahedron, 1998 , vol. 54, # 26 p. 7485 - 7496
反应条件
borane-THF in tetrahydrofuran 14 h; Inert atmosphereReflux;
参考文献
Anastasiadis, Charalampos; Hogarth, Graeme; Wilton-Ely, James D.E.T.
Inorganica Chimica Acta, 2010 , vol. 363, # 13 p. 3222 - 3228
反应条件
sulfuric acid T=40°C; Bei der elektrochemischen Reduktion an einer Zink-Amalgam-Kathode unter Normaldruck,bei 5.3 at und bei 8.5 at;
参考文献
Sakurai
Bl.Fac.lib.Arts Sci.Shinshu Univ., 1955 , # 5 p. Tl.2,S.11,14
反应条件
bei der elektrochemischen Reduktion an einer Blei-Kathode in wss. H2SO4;
参考文献
Dunet et al.
Bulletin de la Societe Chimique de France, 1950 , p. 877,878
反应条件
P=6251.8 Torr; Elektrochemische Reduktion an einer Zink-Amalgam-Kathode;
参考文献
Sakurai
Bulletin of the Chemical Society of Japan, 1932 , vol. 7, p. 155
反应条件
T=18 - 20°C; bei elektrolytischen Reduktion an Bleikathoden,zuletz 60grad;
参考文献
Spaeth; Breusch
Monatshefte fuer Chemie, 1928 , vol. 50, p. 352
参考文献
Uffer; Schlittler
Helvetica Chimica Acta, 1948 , vol. 31, p. 1397,1399
反应条件
[Ni(1,2-bis(di-isopropylphosphino)ethane)(μ-H)]2; hydrogen in tetrahydrofuran T=140°C; P=38787.1 Torr; 72 h; AutoclaveGlovebox;
参考文献
Arevalo, Alma; Ovando-Segovia, Sebastian; Flores-Alamo, Marcos; Garcia, Juventino J.
Organometallics, 2013 , vol. 32, # 10 p. 2939 - 2943
反应条件
hydrogenchloride; hydrazine hydrate in ethanol; N,N-dimethyl-formamide
参考文献
FMC Corporation
Patent: US5683966 A1, 1997 ;
反应条件
Mitsunobu conditions;
参考文献
Tiecco, Marcello; Testaferri, Lorenzo; Temperini, Andrea; Bagnoli, Luana; Marini, Francesca; Santi, Claudio; Terlizzi, Raffaella
European Journal of Organic Chemistry, 2004 , # 16 p. 3447 - 3458
