136918-14-4合成路线 (共 708 条)
反应条件
bis(5-norbornenyl-2-methyl) azodicarboxylate; polystyrene-supported PPh3 in tetrahydrofuran
Substitution; Mitsunobu reaction;
参考文献
Barrett, Anthony G. M.; Roberts, Richard S.; Schroeder, Juergen
Organic Letters, 2000 , vol. 2, # 19 p. 2999 - 3001
反应条件
potassium hydroxide; Aliquatreg; 336 in toluene
T=100°C; 6 h;
参考文献
Santaniello, Enzo; Ponti, Federico
Synthetic Communications, 1980 , vol. 10, # 8 p. 611 - 614
反应条件
in N,N-dimethyl-formamide
参考文献
Krafft, Grant A.; Siddall, Thomas L.
Tetrahedron Letters, 1985 , vol. 26, # 40 p. 4867 - 4870
参考文献
SmithKline Beecham p.l.c.; SmithKline Beecham Corporation
Patent: US6479660 B1, 2002 ;
反应条件
1: phthalimide With potassium hydroxide; Amberlite IRA-400 chloride form
2: ethylene dibromide in tetrahydrofuran
Heating;
参考文献
Dalal; Pawar; Mahulikar
Organic Preparations and Procedures International, 2007 , vol. 39, # 1 p. 81 - 85
反应条件
potassium hydroxide; Aliquatreg; 336 in toluene
T=100°C; 6 h;
参考文献
Santaniello, Enzo; Ponti, Federico
Synthetic Communications, 1980 , vol. 10, # 8 p. 611 - 614
反应条件
potassium tert-butylate in N,N-dimethyl-formamide
1 h; Ambient temperature; Yield given;
参考文献
Fichert, Thomas; Massing, Ulrich
Tetrahedron Letters, 1998 , vol. 39, # 28 p. 5017 - 5018
反应条件
cesium fluoride in N,N-dimethyl-formamide
T=50°C; 7 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Otera, Junzo; Nakazawa, Koichi; Sekoguchi, Koichi; Orita, Akihiro
Tetrahedron, 1997 , vol. 53, # 40 p. 13633 - 13640
反应条件
sodium hydroxide; copper(II) sulfate; zinc in water
3 h; Heating;
参考文献
Cheng, Kur-Ta; Rajasekhar, Dodda; Huang, Sheng-Tung; Hsu, Feng-Lin; Subbaraju, Gottumukkala V.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2003 , vol. 42, # 5 p. 1190 - 1192
反应条件
sodium hydroxide; sodium hypochlorite
参考文献
Mohr; Koehler; Ulrich
Journal fuer Praktische Chemie (Leipzig), 1909 , vol. <2> 80, p. 30