2,5-二甲基-对苯醌合成路线 （共 118 条）
参考文献
Zee-Cheng,K.-Y.; Cheng,C.C.
Journal of Medicinal Chemistry, 1970 , vol. 13, p. 264 - 268
反应条件
1: alcohol; hydroxylamine hydrochloride 2: tin; hydrochloric acid View Scheme
参考文献
Goldschmidt; Schmid
Chemische Berichte, 1885 , vol. 18, p. 570
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Sutkowski
Chemische Berichte, 1887 , vol. 20, p. 979
反应条件
1: alcohol; hydroxylamine hydrochloride 2: tin; hydrochloric acid View Scheme
参考文献
Sutkowski
Chemische Berichte, 1887 , vol. 20, p. 979
反应条件
hydrogenchloride; 4-aminobenzenesulfonic acid
参考文献
Baxter,I.; Titman,R.B.
Journal of the Chemical Society [Section] C: Organic, 1970 , p. 2078 - 2082
参考文献
Carstanjen
Journal fuer Praktische Chemie (Leipzig), 1881 , vol. <2> 23, p. 423,425
Full Text Show Details
Teichner
Chemische Berichte, 1902 , vol. 35, p. 2303
反应条件
1: boron trifluoride diethyl etherate / 40 °C
2: sodium hydroxide / methanol / 23 °C
3: [bis(acetoxy)iodo]benzene
View Scheme
参考文献
Liu, Yanghan; Xiao, Qicai; Liu, Yongqiang; Li, Zheng; Qiu, Yatao; Zhou, Guang-Biao; Yao, Zhu-Jun; Jiang, Sheng
European Journal of Medicinal Chemistry, 2014 , vol. 78, p. 248 - 258
反应条件
1: 72 percent / hydroxylamine hydrochloride / ethanol / 24 h / Heating
2: 71 percent / hydroxylamine hydrochloride / ethanol / 10 h / Heating
3: 92 percent / NO2, O2 / CH2Cl2 / 4 h / Ambient temperature
4: 92 percent / 30percent H2O2 / trifluoroacetic acid / 10 h / Ambient temperature
View Scheme
参考文献
Rathore, R.; Kim, J. S.; Kochi, J. K.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 19 p. 2675 - 2684
参考文献
Ramirez et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 4338,4341
反应条件
boron trifluoride diethyl etherate in dichloromethane
T=-78°C;
参考文献
Naruta, Yoshinori
Journal of the American Chemical Society, 1980 , vol. 102, # 11 p. 3774 - 3783
反应条件
bismuth trifluoromethanesulphonate in dichloromethane
T=20°C; 0.166667 h;
参考文献
Yadav; Reddy; Swamy
Tetrahedron Letters, 2003 , vol. 44, # 26 p. 4861 - 4864
