(±)-2-甲基-1-丁醇合成路线 (共 128 条)
反应条件
phosphorus trichoride
参考文献
Foss
Acta Chemica Scandinavica (1947-1973), 1947 , vol. 1, p. 14
反应条件
Rhizomucor miehei lipase in n-heptane
T=40°C; 24 h; Enzymatic reaction;
参考文献
Divakar, Soundar
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2002 , vol. 41, # 9 p. 1919 - 1922
参考文献
Newton; Walton; Coles; Hodge
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 1995 , vol. 260, # pt 1 p. 107 - 125
反应条件
Rhizomucor miehei lipase in n-heptane
T=40°C; 24 h; Enzymatic reaction;
参考文献
Divakar, Soundar
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2002 , vol. 41, # 9 p. 1919 - 1922
反应条件
(4,5-bis-(di-iso-propylphosphinomethyl)acridine)RuH(CO)Cl; ammonia in toluene
P=5700.38 Torr; 18 h; Inert atmosphereReflux;
参考文献
Gunanathan, Chidambaram; Milstein, David
Angewandte Chemie - International Edition, 2008 , vol. 47, # 45 p. 8661 - 8664
反应条件
1: CuOCr2O3 / 325 - 335 °C
2: KOH-solution
3: iodine / durch Wasserrabspaltung, und Reduktion des entstandenen ungesaettigten Ketons mit Natrium und NaHCO3-Loesung in Aether
View Scheme
参考文献
Powell; Baldwin
Journal of the American Chemical Society, 1936 , vol. 58, p. 1872
参考文献
Lieben; Zeisel
Monatshefte fuer Chemie, 1886 , vol. 7, p. 68
参考文献
Ssuknewitsch; Tschilingarjan
Chemische Berichte, 1935 , vol. 68, p. 1211,1216
Chemische Berichte, 1936 , vol. 69, p. 1538,1539,1541,1542