1-苯基癸-1,3-二酮合成路线 （共 42 条）
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=20°C; Substitution;
参考文献
Zhong; Xiong; Huang
Synthetic Communications, 2000 , vol. 30, # 19 p. 3535 - 3541
反应条件
sodium acetate; palladium diacetate in N,N-dimethyl acetamide T=125°C; 16 h;
参考文献
Bagnell; Kreher; Strauss
Chemical Communications, 2001 , # 1 p. 29 - 30
反应条件
RhH(CO)(triphenylphosphine)3; hydrogen; triphenylphosphine in benzene T=80°C; P=20685.9 Torr; 20 h;
参考文献
Australian Journal of Chemistry, , vol. 42, # 4 p. 471 - 478
参考文献
Chemische Berichte, , vol. 66, p. 389,391
反应条件
palladium diacetate; tributyl-amine; tributylphosphine in tert-butyl alcohol 48 h; Heating;
参考文献
Kim, Ji-Hyun; Kulawiec, Robert J.
Journal of Organic Chemistry, 1996 , vol. 61, # 22 p. 7656 - 7657
反应条件
1: meso-1,2-diphenylethylene With N,N,N',N'',N''-pentamethyldiethylenetriamine; sec.-butyllithium in tetrahydrofuran T=-25°C; 2 h; 2: N,N-dimethyl-formamide in tetrahydrofuran T=-25 - 20°C; 3: With hydrogenchloride in tetrahydrofuran Further stages.;
参考文献
Organic Letters, , vol. 9, # 8 p. 1493 - 1496
反应条件
hydrogen; dodecacarbonyltetrarhodium(0)
参考文献
Tetrahedron Letters, , vol. 27, # 37 p. 4497 - 4500
反应条件
C34H51NP2; hydrogen; palladium (II) 2,4-pentanedionate; toluene-4-sulfonic acid in tetrahydrofuran T=80°C; P=37503.8 Torr; 20 h; Schlenk techniqueAutoclaveInert atmosphere; stereoselective reaction;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 17 p. 4645 - 4649
反应条件
C34H51NP2; hydrogen; palladium (II) 2,4-pentanedionate; toluene-4-sulfonic acid in tetrahydrofuran T=80°C; P=37503.8 Torr; 20 h; Schlenk techniqueAutoclaveInert atmosphere; stereoselective reaction;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 17 p. 4645 - 4649
反应条件
1: 31 percent / LDA / tetrahydrofuran / 0.08 h / -78 °C 2: TMSOTf / CH2Cl2 / 5 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 66, # 6 p. 2149 - 2153
