二乙基三甲基硅基亚磷酸酯合成路线 (共 88 条)
反应条件
tin(IV) chloride in dichloromethane 3 h; 0 deg C -> room temperature;
参考文献
Kim, Dae Young; Oh, Dong Young
Synthetic Communications, 1986 , vol. 16, # 8 p. 859 - 864
参考文献
Prishchenko, Andrey A.; Livantsov, Mikhail V.; Novikova, Olga P.; Livantsova, Ludmila I.; Petrosyan, Valery S.
Heteroatom Chemistry, 2012 , vol. 23, # 4 p. 352 - 372
参考文献
Prishchenko, Andrey A.; Livantsov, Mikhail V.; Novikova, Olga P.; Livantsova, Ludmila I.; Petrosyan, Valery S.
Heteroatom Chemistry, 2012 , vol. 23, # 4 p. 352 - 372
反应条件
T=-80°C; P=50 Torr; 3 h;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 52, # 4 p. 769 - 776,667 - 673
参考文献
Malenko, D. M.; Gololobov, Yu. G.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 6 p. 1432 - 1433,1214 - 1215
反应条件
hydrogenchloride various electrophilic initiators; Mechanism;
参考文献
Nesterov, L. V.; Aleksandrova, N. A.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 1 p. 222 - 223,195 - 196
反应条件
in dichloromethane or in benzene;
参考文献
Afarinkia, Kamyar; Rees, Charles W.; Cadogan, John I. G.
Tetrahedron, 1990 , vol. 46, # 20 p. 7175 - 7196
反应条件
trichloroacetonitrile in pentane T=20°C; 0.5 h;
参考文献
Lermontov, S. A.; Zavorin, S. I.; Sukhozhenko, I. I.; Pushin, A. N.; Martynov, I. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 2.2 p. 404 - 408
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , vol. 40, # 2 p. 468 - 472
反应条件
in neat (no solvent) T=150°C; 1.5 h;
参考文献
Lermontov, S. A.; Zavorin, S. I.; Sukhozhenko, I. I.; Pushin, A. N.; Martynov, I. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 2.2 p. 404 - 408
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , vol. 40, # 2 p. 468 - 472
反应条件
T=20 - 25°C; 1) hexane 2) without solvent; Yield given. Yields of byproduct given;
参考文献
Kutyrev, A. A.; Moskva, V. V.; Alparova, M. V.
J. Gen. Chem. USSR (Engl. Transl.), 1984 , vol. 54, # 7 p. 1494 - 1499,1332 - 1336