二乙基三甲基硅基亚磷酸酯合成路线 （共 88 条）
反应条件
ClSO2F (sulfuryl chloride fluoride) in dichloromethane a) -50 deg C, 1 h, b) 20 deg C, 1 h;
参考文献
Dabkowski, Wojciech; Cramer, Friedrich; Michalski, Jan
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 11 p. 1447 - 1452
反应条件
10 h; Ambient temperature;
参考文献
Lermontov, S. A.; Rakov, I. M.; Martynov, I. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 2 p. 1978
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , vol. 9, p. 2149 - 2150
参考文献
Novikova,Z.S.; Lutsenko,I.F.
J. Gen. Chem. USSR (Engl. Transl.), 1970 , vol. 40, # 9 p. 2129,2110
反应条件
T=150°C; 6 h; Mechanism;
参考文献
Gazizov, T. Kh.; Sudarev, Yu. I.; Shakirov, I. Kh.; Smirnov, V. N.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 4 p. 769 - 776,667 - 673
反应条件
sodium perchlorate electrolysis;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 53, # 1 p. 233,204
反应条件
phosphonic acid diethyl ester in dichloromethane Inert atmosphere;
参考文献
Prishchenko, Andrey A.; Livantsov, Mikhail V.; Novikova, Olga P.; Livantsova, Ludmila I.; Petrosyan, Valery S.
Heteroatom Chemistry, 2013 , vol. 24, # 4 p. 332 - 335
反应条件
boron trifluoride diethyl etherate 1.) THF, -10 deg C, 5 min.; 2.) TBAF, from -10 to RT; Yield given. Multistep reaction;
参考文献
Ku, Bonchul; Oh, Dong Young
Tetrahedron Letters, 1988 , vol. 29, # 35 p. 4465 - 4466
参考文献
Kamalov, R. M.; Stepanov, G. S.; Pudovik, M. A.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 2.2 p. 476 - 477,414 - 415
反应条件
in diethyl ether
16 h; Heating;
参考文献
Creary, Xavier; Geiger, Cristina C.; Hilton, Kathryn
Journal of the American Chemical Society, 1983 , vol. 105, # 9 p. 2851 - 2858
反应条件
chloro-trimethyl-silane; triethylamine in diethyl ether
参考文献
Bayer Corporation
Patent: US5886022 A1, 1999 ;
US 5886022 A
