二乙基三甲基硅基亚磷酸酯合成路线 (共 88 条)
反应条件
in diethyl ether
Yield given;
参考文献
Kutyrev, G. A.; Kutyrev, A. A.; Cherkasov, R. A.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 12 p. 2738 - 2745,2216 - 2222
参考文献
Pudovik, M. A.; Kibardina, L. K.; Pudovik, A. N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 1.2 p. 214 - 216
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , # 1 p. 232 - 235
反应条件
T=150°C; P=30 Torr; 3 h; Mechanism;
参考文献
Sekine, Mitsuo; Nakajima, Masashi; Hata, Tsujiaki
Journal of Organic Chemistry, 1981 , vol. 46, # 20 p. 4030 - 4034
反应条件
(i) Na, Et2O, (ii) /BRN= 1731135/; Multistep reaction;
参考文献
Bugerenko,E.F. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1966 , p. 1334 - 1337
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1966 , p. 1391 - 1396
参考文献
Pudovik,M.A. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1975 , vol. 45, p. 700,682
参考文献
Pudovik, M. A.; Kibardina, L. K.; Pudovik, A. N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 1.2 p. 217 - 218
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , # 1 p. 235 - 237
反应条件
(i) (heating), (ii) EtOH; Multistep reaction;
参考文献
Novikova,Z.S. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1971 , vol. 41, p. 2622 - 2628,2655 - 2660
反应条件
zinc(II) chloride
T=130°C;
参考文献
Prishchenko, Andrey A.; Livantsov, Mikhail V.; Novikova, Olga P.; Livantsova, Ludmila I.; Petrosyan, Valery S.
Heteroatom Chemistry, 2009 , vol. 20, # 6 p. 319 - 324
反应条件
reaction with other silylphosphites investigated;
参考文献
Nesterov, L. V.; Krepysheva, N. E.; Aleksandrova, N. A.
J. Gen. Chem. USSR (Engl. Transl.), 1989 , vol. 59, # 3.2 p. 725,641
反应条件
tin(IV) chloride in dichloromethane
3 h; 0 deg C -> room temperature;
参考文献
Kim, Dae Young; Oh, Dong Young
Synthetic Communications, 1986 , vol. 16, # 8 p. 859 - 864