二乙基三甲基硅基亚磷酸酯合成路线 (共 88 条)
反应条件
benzaldehyde in methanol
参考文献
The Upjohn Company
Patent: US5500417 A1, 1996 ;
反应条件
T=45 - 55°C; 3 h; Product distribution;
参考文献
Gazizov, T. Kh.; Ustanova, L. N.; Ryzhikov, D. V.; Pudovik, A. N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 1673 - 1674
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 8 p. 1830 - 1832
反应条件
zinc(II) chloride
T=130°C; 1 h; Inert atmosphere;
参考文献
Prishchenko, Andrey A.; Livantsov, Mikhail V.; Novikova, Olga P.; Livantsova, Ludmila I.; Petrosyan, Valery S.
Heteroatom Chemistry, 2010 , vol. 21, # 2 p. 71 - 77
反应条件
zinc(II) iodide
T=55 - 60°C; 1 h;
参考文献
Azuhata, Toshio; Okamoto, Yoshiki
Synthesis, 1983 , # 11 p. 916 - 917
反应条件
zinc(II) chloride
T=110 - 130°C; 2 h;
参考文献
Prishchenko, Andrey A.; Livantsov, Mikhail V.; Novikova, Olga P.; Livantsova, Ludmila I.; Petrosyan, Valery S.
Heteroatom Chemistry, 2008 , vol. 19, # 5 p. 450 - 454
参考文献
Sekine, Mitsuo; Nakajima, Masashi; Kume, Akiko; Hashizume, Akio; Hata, Tsujiaki
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 1 p. 224 - 238
反应条件
tin(IV) chloride in dichloromethane
2.5 h; 0 deg C -> room temperature;
参考文献
Kim, Dae Young; Oh, Dong Young
Synthetic Communications, 1986 , vol. 16, # 8 p. 859 - 864
反应条件
tin(IV) chloride in dichloromethane
2.5 h; 0 deg C -> room temperature;
参考文献
Kim, Dae Young; Oh, Dong Young
Synthetic Communications, 1986 , vol. 16, # 8 p. 859 - 864
反应条件
zinc(II) chloride
T=90°C; 1.5 h;
参考文献
Prishchenko, A.A.; Livantsov, M.V.; Petrosyan, V.S.
Russian Journal of General Chemistry, 1994 , vol. 64, # 8.2 p. 1181 - 1193
Zhurnal Obshchei Khimii, 1994 , vol. 64, # 8 p. 1316 - 1330
参考文献
Gazizov, T. Kh.; Ustanova, L. N.; Ryzhikov, D. V.; Pudovik, A. N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 1673 - 1674
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 8 p. 1830 - 1832