二乙基三甲基硅基亚磷酸酯合成路线 （共 88 条）
反应条件
in 1,2-dichloro-ethane
Heating;
参考文献
Afarinkia, Kamyar; Rees, Charles W.; Cadogan, John I. G.
Tetrahedron, 1990 , vol. 46, # 20 p. 7175 - 7196
反应条件
toluene-4-sulfonic acid; tin(ll) chloride
1.) 60 deg C, 1 h, 2.) EtOH, 60 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Courtois; Miginiac
Synthetic Communications, 1991 , vol. 21, # 2 p. 201 - 209
反应条件
bromine
T=-60 - -40°C; 6 h; solvent (CH2Cl2) was used as well;
参考文献
Gazizov, T. Kh.; Sudarev, Yu. I.; Shakirov, I. Kh.; Smirnov, V. N.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 4 p. 769 - 776,667 - 673
参考文献
Pudovik,A.N. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1974 , vol. 44, # 3 p. 522 - 526,500 - 503
反应条件
T=45 - 55°C; 3 h; Product distribution;
参考文献
Gazizov, T. Kh.; Ustanova, L. N.; Ryzhikov, D. V.; Pudovik, A. N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 1673 - 1674
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 8 p. 1830 - 1832
反应条件
T=80 - 100°C; P=50 Torr; 3 h;
参考文献
Gazizov, T. Kh.; Sudarev, Yu. I.; Shakirov, I. Kh.; Smirnov, V. N.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 4 p. 769 - 776,667 - 673
反应条件
T=20 - 25°C; 1) hexane 2) without solvent; Yield given. Yields of byproduct given;
参考文献
Kutyrev, A. A.; Moskva, V. V.; Alparova, M. V.
J. Gen. Chem. USSR (Engl. Transl.), 1984 , vol. 54, # 7 p. 1494 - 1499,1332 - 1336
反应条件
T=45 - 55°C; 3 h; Product distribution;
参考文献
Gazizov, T. Kh.; Ustanova, L. N.; Ryzhikov, D. V.; Pudovik, A. N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 1673 - 1674
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 8 p. 1830 - 1832
