1-苯基-1-三甲基甲硅氧基乙烯合成路线 (共 431 条)
反应条件
potassium fluoride; oxygen; isobutyraldehyde; bis(3-methyl-2,4-pentanedionato)nickel(II) 1.) 1,2-dichloroethane, RT, 6 h, 2.) MeOH; Yield given. Multistep reaction;
参考文献
Takai, Toshihiro; Yamada, Tohru; Rhode, Oliver; Mukaiyama, Teruaki
Chemistry Letters, 1991 , # 2 p. 281 - 284
反应条件
3-chloro-benzenecarboperoxoic acid
参考文献
Klis; Erhardt
Synthetic Communications, 2000 , vol. 30, # 22 p. 4027 - 4038
反应条件
oxygen in chlorobenzene T=95°C; 5.9 h; var. of temp., solvent, addition of cumene hydroperoxide, ΔEA; Product distributionThermodynamic dataKinetics;
参考文献
Suprun
Journal fuer Praktische Chemie - Practical Applications and Applied Chemistry (Germany), 1999 , vol. 341, # 1 p. 52 - 58
反应条件
potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)); Tedicyp in N,N-dimethyl-formamide T=130°C; Heck reaction; 20 h;
参考文献
Battace, Ahmed; Feuerstein, Marie; Lemhadri, Mhamed; Zair, Touriya; Doucet, Henri; Santelli, Maurice
European Journal of Organic Chemistry, 2007 , # 19 p. 3122 - 3132
反应条件
chloromethyl iodide in dimethyl sulfoxide 3 h; Ambient temperature;
参考文献
Miyano, Sotaro; Hokari, Hiroshi; Mori, Akira; Hashimoto, Harukichi
Chemistry Letters, 1980 , p. 1213 - 1214
反应条件
stannous bromide in dichloromethane 1.5 h; Ambient temperature;
参考文献
Hayashi, Masaji; Mukaiyama, Teruaki
Chemistry Letters, 1987 , p. 1283 - 1286
参考文献
Graven, Anette; Grotli, Morten; Meldal, Morten
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 6 p. 955 - 962
反应条件
lead(IV) acetate in tetrahydrofuran; dichloromethane T=-78 - -25°C; 2.5 h; 1) -78 degC, 1.5h 2) R.T., 1h;
参考文献
Moriarty, Robert M.; Penmasta, Raju; Prakash, Indra
Tetrahedron Letters, 1987 , vol. 28, # 8 p. 873 - 876
反应条件
1: 65 percent / CH2Cl2 / 5 h / Ambient temperature 2: 90 percent / boron trifluoride etherate / 5 h / Ambient temperature View Scheme
参考文献
Brunovlenskaya, I. I.; Kusainova, K. M.; Kashin, A. K.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 2 p. 316 - 320
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 2 p. 358 - 363
反应条件
lead(IV) acetate; 4-tolylthallium(III) bis(trifluoroacetate) 1.) benzene, RT, 30 min, 2.) RT; Yield given. Multistep reaction;
参考文献
Moriarty, Robert M.; Penmasta, Raju; Prakash, Indra; Awasthi, Alok K.
Journal of Organic Chemistry, 1988 , vol. 53, # 5 p. 1022 - 1025