1-苯基-1-三甲基甲硅氧基乙烯 合成路线 (共 431 条)
反应条件
1: 1.) MeLi / 1.) THF, ether, 0 deg C, 30 min, 2.) THF, ether, CH2Cl2, hexane, -78 deg C, 0.5 h 2: 95 percent / 1,3,5-trimethyl-benzene / 7.5 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 115, # 10 p. 3943 - 3949
反应条件
sodium hydroxide; formic acid; water; sodium chloride in acetonitrile T=25°C; Rate constantMechanism;
参考文献
Novice, Marilyn H.; Seikaly, Hani R.; Seiz, Annette D.; Tidwell, Thomas T.
Journal of the American Chemical Society, 1980 , vol. 102, # 18 p. 5835 - 5838
反应条件
ClSO2F (sulfuryl chloride fluoride) in dichloromethane 1) -78 deg C, 2) RT, 30 min;
参考文献
Journal of Organic Chemistry, , vol. 49, # 11 p. 2032 - 2034
反应条件
ruthenium (2+) in benzene T=120°C; 7 h; sealed;
参考文献
Journal of Organometallic Chemistry, , vol. 552, # 1-2 p. 39 - 43
55591-23-6 1,1,2,2,3,3,4,4,5,5,6,6,6-十三氟己烷-1-磺酰氯
→
反应条件
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in benzene T=120°C; 7 h;
参考文献
Phosphorus, Sulfur and Silicon and Related Elements, , vol. 129, p. 155 - 168
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in benzene T=120°C; 7 h;
参考文献
Phosphorus, Sulfur and Silicon and Related Elements, , vol. 129, p. 155 - 168
反应条件
TNM in pentane 6 h; Ambient temperature;
参考文献
Rathore, Rajendra; Lin, Zhe; Kochi, Jay K.
Tetrahedron Letters, 1993 , vol. 34, # 12 p. 1859 - 1862
反应条件
in dichloromethane 6 h; Ambient temperature;
参考文献
Rathore, Rajendra; Kochi, Jay K.
Journal of Organic Chemistry, 1996 , vol. 61, # 2 p. 627 - 639
反应条件
antimony trichloride in dichloromethane T=0°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 47, # 26 p. 5099 - 5102
反应条件
antimony trichloride in dichloromethane T=0°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 47, # 26 p. 5099 - 5102