1-苯基-1-三甲基甲硅氧基乙烯合成路线 (共 431 条)
反应条件
lithium bromide in diethyl ether T=-78°C; another reagent;
参考文献
Creary, Xavier
Journal of Organic Chemistry, 1980 , vol. 45, # 13 p. 2727 - 2729
反应条件
potassium tert-butylate
参考文献
Katritzky, Alan R.; Hayden, Amy E.; Kirichenko, Kostyantyn; Pelphrey, Phillip; Ji, Yu
Journal of Organic Chemistry, 2004 , vol. 69, # 15 p. 5108 - 5111
反应条件
iodosylbenzene; boron trifluoride diethyl etherate in dichloromethane T=-40 - 20°C; 2.5 h;
参考文献
Dae Young Kim; Joo Yang Mang; Dong Young Oh
Synthetic Communications, 1994 , vol. 24, # 5 p. 629 - 634
反应条件
(CF3SO2)2NSiMe3 in dichloromethane T=-78°C; Sakurai-Hosomi allylation; 0.25 h;
参考文献
Ishihara; Hiraiwa; Yamamoto
Synlett, 2001 , # 12 p. 1851 - 1854
反应条件
lt;Ru(PPh3)3Cl2gt; in benzene T=120°C; 7 h;
参考文献
Kamigata, Nobumasa; Udodaira, Kumiko; Shimizu, Toshio
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 5 p. 783 - 786
反应条件
[Mo(.mu.-Cl)(SnCl3)(CO)3(NCCH3)2] in dichloromethane 2 h; Ambient temperature;
参考文献
Malkov, Andrei V.; Baxendale, Ian R.; Dvorak, Dalimil; Mansfield, Darren J.; Kocovsky, Pavel
Journal of Organic Chemistry, 1999 , vol. 64, # 8 p. 2737 - 2750
反应条件
silver trifluoromethanesulfonate in dichloromethane 2 h; Ambient temperature;
参考文献
Takeda, Kazuyoshi; Torii, Katsumi; Ogura, Haruo
Tetrahedron Letters, 1990 , vol. 31, # 2 p. 265 - 266
反应条件
1: CH2Cl2 / -78 °C 2: 90 percent / CH2Cl2 / 0.17 h / Ambient temperature View Scheme
参考文献
Zhdankin, Viktor V.; Tykwinski, Rik; Caple, Roland; Berglund, Bruce; Koz'min, Anatoly S.; Zefirov, Nikolai S.
Tetrahedron Letters, 1988 , vol. 29, # 30 p. 3703 - 3704
反应条件
iron(III) chloride in acetonitrile T=20°C; 0.0833333 h;
参考文献
Zhan, Zhuang-Ping; Wang, Shao-Pei; Cai, Xu-Bin; Liu, Hui-Juan; Yu, Jing-Liang; Cui, Yuan-Yuan
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 13 p. 2097 - 2102
反应条件
potassium tert-butylate
参考文献
Katritzky, Alan R.; Hayden, Amy E.; Kirichenko, Kostyantyn; Pelphrey, Phillip; Ji, Yu
Journal of Organic Chemistry, 2004 , vol. 69, # 15 p. 5108 - 5111