1-苯基-1-三甲基甲硅氧基乙烯合成路线 (共 431 条)
反应条件
[(tris(1-pyrazolyl)borate)Ru(P(phenyl)3)(CH3CN)2]PF6
T=100°C; 15 h;
参考文献
Odedra, Arjan; Wu, Chang-Jung; Pratap, Taduri Bhanu; Huang, Chun-Wei; Ran, Ying-Fen; Liu, Rai-Shung
Journal of the American Chemical Society, 2005 , vol. 127, # 10 p. 3406 - 3412
反应条件
1: in xylene
T=25°C; 3 h;
2: in xylene
3 h; Heating; Further stages.;
参考文献
Akbas; Sonmez; Anil; Aslanoglu
Russian Journal of General Chemistry, 2008 , vol. 78, # 6 p. 1277 - 1282
反应条件
titanium tetrachloride; triethylamine; trifluoroacetic anhydride
Yield given. Multistep reaction;
参考文献
Bouhlel; Hassine
Synthetic Communications, 1992 , vol. 22, # 15 p. 2183 - 2186
反应条件
oxygen in chlorobenzene
T=95°C; 5.9 h; var. of temp., solvent, addition of cumene hydroperoxide, ΔEA; Product distributionThermodynamic dataKinetics;
参考文献
Suprun
Journal fuer Praktische Chemie - Practical Applications and Applied Chemistry (Germany), 1999 , vol. 341, # 1 p. 52 - 58
反应条件
ytterbium(III) triflate in tetrahydrofuran; dichloromethane
T=0 - 20°C; Condensation; aldol reaction; 2.5 h;
参考文献
Graven, Anette; Grotli, Morten; Meldal, Morten
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 6 p. 955 - 962
反应条件
1: With trifluorormethanesulfonic acid in acetonitrile
T=20°C; 3 h;
2: With manganese triacetate in acetic acid; acetonitrile
T=20°C; 24 h;
参考文献
Akiyama, Takahiko; Nakashima, Saeko; Yokota, Koji; Fuchibe, Kohei
Chemistry Letters, 2004 , vol. 33, # 7 p. 922 - 923
反应条件
antimony trichloride in dichloromethane
T=0°C; 1 h;
参考文献
Tirpak, Robin E.; Rathke, Michael W.
Journal of Organic Chemistry, 1982 , vol. 47, # 26 p. 5099 - 5102
反应条件
antimony trichloride in dichloromethane
T=0°C; 1 h;
参考文献
Tirpak, Robin E.; Rathke, Michael W.
Journal of Organic Chemistry, 1982 , vol. 47, # 26 p. 5099 - 5102
反应条件
bismuth(III) chloride; sodium iodide in diethyl ether; dichloromethane
0.666667 h; Ambient temperature;
参考文献
Le Roux, Christophe; Mandrou, Stephanie; Dubac, Jacques
Journal of Organic Chemistry, 1996 , vol. 61, # 11 p. 3885 - 3887
反应条件
[1,1'-bis(diphenylphosphino)ferrocene]dichloronickel (II)
1.) ether, room temp., 2.) benzene, reflux; Yield given. Multistep reaction;
参考文献
Hayashi, Tamio; Katsuro, Yoshio; Kumada, Makoto
Tetrahedron Letters, 1980 , vol. 21, p. 3915 - 3918