1-苯基-1-三甲基甲硅氧基乙烯合成路线 （共 431 条）
反应条件
bis(acetylacetonate)nickel(II) in diethyl ether
Heating;
参考文献
Hayashi, Tamio; Katsuro, Yoshio; Kumada, Makoto
Tetrahedron Letters, 1980 , vol. 21, p. 3915 - 3918
反应条件
bis(acetylacetonate)nickel(II) in diethyl ether
Heating;
参考文献
O'Neill; Pugh; Stachulski; Ward; Davies; Kevin Park
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 20 p. 2682 - 2689
反应条件
diethylaluminium chloride in hexane; dichloromethane
1.) -78 deg C, 30 min, 2.) 20 deg C, 1 h;
参考文献
Matsumura, Yasushi; Fujiwara, Junya; Maruoka, Keiji; Yamamoto, Hisashi
Journal of the American Chemical Society, 1983 , vol. 105, # 20 p. 6312 - 6314
反应条件
boron trifluoride diethyl etherate; triphenylbismuth(V) difluoride
1.) CH2Cl2, room temperature, 10 h, 2.) room temperature, 6 h; Yield given. Multistep reaction;
参考文献
Matano, Yoshihiro; Azuma, Nagao; Suzuki, Hitomi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 13 p. 1739 - 1748
反应条件
sodium hydroxide; tetrabutylammomium bromide in dichloromethane
8 h; Ambient temperature;
参考文献
Swamy, Vishwanath M.; Sarkar, Amitabha
Tetrahedron Letters, 1998 , vol. 39, # 10 p. 1261 - 1264
反应条件
1: 3-phenyl-propenal With N,N-bis(perfluoromethanesulfonyl)squaramide in acetonitrile
T=20°C; 0.166667 h; Inert atmosphere;
2: [(1-phenyl-1-ethenyl)oxy]trimethylsilane in acetonitrile
T=20°C; Mukaiyama aldol reaction; 2 h; Inert atmosphere;
3: With hydrogenchloride; water
T=20°C; Mukaiyama aldol reaction; 0.5 h; Inert atmosphere;
参考文献
Cheon, Cheol Hong; Yamamoto, Hisashi
Tetrahedron, 2010 , vol. 66, # 24 p. 4257 - 4264
反应条件
1: (2R,3R)-2-(2,6-diisopropoxybenzoyloxy)-3-hydroxybutanedioic acid, BH3*THF / tetrahydrofuran; various solvent(s) / 2 h / -78 °C
2: 1 N HCl / tetrahydrofuran
View Scheme
参考文献
Furuta, Kyoji; Maruyama, Tohru; Yamamoto, Hisashi
Journal of the American Chemical Society, 1991 , vol. 113, # 3 p. 1041 - 1042
反应条件
1: With boron trifluoride diethyl etherate in dichloromethane
0.416667 h; Inert atmosphere;
2: With ammonium cerium (IV) nitrate; triethylamine in acetone
Inert atmosphere;
参考文献
Kusama, Hiroyuki; Ishida, Kento; Funami, Hideaki; Iwasawa, Nobuharu
Angewandte Chemie - International Edition, 2008 , vol. 47, # 26 p. 4903 - 4905
反应条件
indium(III) chloride in water
T=23°C; 15 h;
参考文献
Loh, Teck-Peng; Pei, Jian; Cao, Guo-Qiang
Chemical Communications, 1996 , # 15 p. 1819 - 1820
反应条件
1: 73 percent / ZnBr2 / CH2Cl2 / 48 h / Ambient temperature
2: 1.) Ra-Ni, 2.) PCC / 1.) EtOH, 70 deg C, 4 h, rt, 20 h, 2.) CH2Cl2
View Scheme
参考文献
Pohmakotr, Manat; Thisayukta, Jirakorn
Tetrahedron Letters, 1997 , vol. 38, # 38 p. 6759 - 6762
