1-苯基-1-三甲基甲硅氧基乙烯合成路线 （共 431 条）
反应条件
1: ortho-anisaldehyde With N,N-bis(perfluoromethanesulfonyl)squaramide in acetonitrile
T=20°C; 0.166667 h; Inert atmosphere;
2: [(1-phenyl-1-ethenyl)oxy]trimethylsilane in acetonitrile
T=20°C; Mukaiyama aldol reaction; 2 h; Inert atmosphere;
3: With hydrogenchloride; water
T=20°C; Mukaiyama aldol reaction; 0.5 h; Inert atmosphere;
参考文献
Cheon, Cheol Hong; Yamamoto, Hisashi
Tetrahedron, 2010 , vol. 66, # 24 p. 4257 - 4264
反应条件
1: mischmetall tribromide*(thf)x / CH2Cl2 / 3 h / 20 °C
2: aq. HCl / tetrahydrofuran / 2 h / 20 °C
View Scheme
参考文献
Lannou, Marie-Isabelle; Helion, Florence; Namy, Jean-Louis
Tetrahedron, 2003 , vol. 59, # 52 p. 10551 - 10565
反应条件
1: 90 percent / BiCl3-3 NaI / CH2Cl2 / 0.25 h / Ambient temperature
2: 1N HCl / methanol; H2O / Ambient temperature
View Scheme
参考文献
Roux, C. Le; Gaspard-Iloughmane, H.; Dubac, J.
Bulletin de la Societe Chimique de France, 1993 , vol. 130, p. 832 - 842
反应条件
silver perchlorate; diphenyltin sulfide in dichloromethane
T=-78°C; 3 h;
参考文献
Mukaiyama, Teruaki; Saito, Katsuyuki; Kitagawa, Hideo; Shimomura, Naoyuki
Chemistry Letters, 1994 , # 4 p. 789 - 792
反应条件
bis-(pentafluoro phenyl) dibromo stannane in dichloromethane
T=-78°C; parallel recognition; 5 h;
参考文献
Chen, Jian-Xie; Sakamoto, Katsumasa; Orita, Akihiro; Otera, Junzo
Tetrahedron, 1998 , vol. 54, # 29 p. 8411 - 8420
反应条件
(C6F5)SnBr2 in dichloromethane
T=-78°C; parallel recognition; 5 h;
参考文献
Chen, Jian-Xie; Sakamoto, Katsumasa; Orita, Akihiro; Otera, Junzo
Tetrahedron, 1998 , vol. 54, # 29 p. 8411 - 8420
反应条件
bis-(pentafluoro phenyl) dibromo stannane in dichloromethane
T=-78°C; parallel recognition; 5 h;
参考文献
Chen, Jian-Xie; Sakamoto, Katsumasa; Orita, Akihiro; Otera, Junzo
Tetrahedron, 1998 , vol. 54, # 29 p. 8411 - 8420
反应条件
bis-(pentafluoro phenyl) dibromo stannane in dichloromethane
T=-78°C; parallel recognition; 5 h;
参考文献
Chen, Jian-Xie; Sakamoto, Katsumasa; Orita, Akihiro; Otera, Junzo
Tetrahedron, 1998 , vol. 54, # 29 p. 8411 - 8420
反应条件
bis-(pentafluoro phenyl) dibromo stannane in dichloromethane
T=-78°C; parallel recognition; 5 h;
参考文献
Chen, Jian-Xie; Sakamoto, Katsumasa; Orita, Akihiro; Otera, Junzo
Tetrahedron, 1998 , vol. 54, # 29 p. 8411 - 8420
反应条件
titanium tetrachloride in dichloromethane
T=-78°C; parallel recognition; 5 h;
参考文献
Chen, Jian-Xie; Sakamoto, Katsumasa; Orita, Akihiro; Otera, Junzo
Tetrahedron, 1998 , vol. 54, # 29 p. 8411 - 8420
