反应条件
hydrogen iodide in diethyl ether; n-heptane byproducts: LiCl, B2H6, H2; (Ar); ZrCl4 and LiBH4 were shaken in a Schlenk tube, dissolving in n-heptane at -78°C in vacuo, HBr was bubbled for 6 h at ambient temp.,stirring 12 h under HBr atmosphere; filtn., washed with n-heptane, dried in vacuo, sublimed at 170°C for 15 h, elem. anal.;
参考文献
Calderazzo, Fausto; Pallavicini, Piersandro; Pampaloni, Guido
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1990 , # 6 p. 1813 - 1818
