in toluene under N2 or Ar; SbF3 and toluene stirred at -78°C; soln. of (HNBCl)3 in toluene added dropwise; warmed to ambient temp.; filtered; filtrate stored at -25°C for 1 d;
参考文献
Anand, Benadir; Noeth, Heinrich; Schwenk-Kircher, Holger; Troll, Alexander
European Journal of Inorganic Chemistry, 2008 , # 20 p. 3186 - 3199