alpha-乙酰氧基-(3,4-二甲氧基苯基)乙腈合成路线 (共 5 条)
反应条件
1: trimethylsilyl cyanide; 3,4-dimethoxy-benzaldehyde With lithium boron tetrafluoride in dichloromethane; acetonitrile T=23°C; 0.5 h; 2: acetic anhydride in dichloromethane; acetonitrile T=23°C; 2.5 h; Further stages.;
参考文献
Yadav; Reddy, B.V. Subba; Vishnumurthy; Chary, Ch. Janardhana
Tetrahedron Letters, 2007 , vol. 48, # 33 p. 5915 - 5918
反应条件
T=20°C; Cooling with iceInert atmosphere;
参考文献
Kumaraswamy; Ankamma
Organic Preparations and Procedures International, 2008 , vol. 40, # 5 p. 447 - 455
参考文献
Kindler
Archiv der Pharmazie (Weinheim, Germany), 1931 , vol. 269, p. 70,76
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Hahn; Rumpf
Chemische Berichte, 1938 , vol. 71, p. 2141,2147
Full Text Show Details
Hahn; Stiehl; Schulz
Chemische Berichte, 1939 , vol. 72, p. 1291,1296
反应条件
sulfuric acid; palladium; acetic acid Hydrogenation;
参考文献
Archiv der Pharmazie (Weinheim, Germany), , vol. 269, p. 70,76
参考文献
Archiv der Pharmazie (Weinheim, Germany), , vol. 269, p. 70,76