反应条件
perchloric acid in sulfolane
Co complex in sulfolane and isoxazole reacting in sulfolane at room temp. for 15 h, adding to 2-butanol in Et2O, solid sepg., dissolving in H2O, treating with HClO4, cooling, by-product filtering off, filtrate treating with conc. HClO4, ppt. sepg.; identified by elem. anal., IR, UV and NMR spectra;
参考文献
Kupferschmidt, W. C.; Jordan, R.B.
Inorganic Chemistry, 1982 , vol. 21, p. 2089 - 2091