4-甲氧苯基3-O-苄基-2-脱氧-2-苯二甲酰亚氨基-Β-D-吡喃葡萄糖苷合成路线 （共 6 条）
反应条件
toluene-4-sulfonic acid in 1,4-dioxane; methanol 1) 1 h, 60 deg C, 2) 45 min, 85 deg C;
参考文献
Nakano; Ito; Ogawa
Carbohydrate Research, 1993 , vol. 243, # 1 p. 43 - 69
反应条件
1: 84 percent / Me3SiOTf / 1,2-dichloro-ethane / 3 h / 0 °C 2: p-TsOH*H2O / dimethylformamide / 20 h / 20 °C 3: 61 percent / NaH / dimethylformamide / 20 h / 20 °C 4: 77 percent / p-TsOH*H2O / methanol; dioxane / 1) 1 h, 60 deg C, 2) 45 min, 85 deg C View Scheme
参考文献
Nakano; Ito; Ogawa
Carbohydrate Research, 1993 , vol. 243, # 1 p. 43 - 69
反应条件
1: 61 percent / NaH / dimethylformamide / 20 h / 20 °C 2: 77 percent / p-TsOH*H2O / methanol; dioxane / 1) 1 h, 60 deg C, 2) 45 min, 85 deg C View Scheme
参考文献
Nakano; Ito; Ogawa
Carbohydrate Research, 1993 , vol. 243, # 1 p. 43 - 69
反应条件
1: p-TsOH*H2O / dimethylformamide / 20 h / 20 °C 2: 61 percent / NaH / dimethylformamide / 20 h / 20 °C 3: 77 percent / p-TsOH*H2O / methanol; dioxane / 1) 1 h, 60 deg C, 2) 45 min, 85 deg C View Scheme
参考文献
Nakano; Ito; Ogawa
Carbohydrate Research, 1993 , vol. 243, # 1 p. 43 - 69
反应条件
1: 84 percent / Me3SiOTf / 1,2-dichloro-ethane / 3 h / 0 °C 2: p-TsOH*H2O / dimethylformamide / 20 h / 20 °C 3: 61 percent / NaH / dimethylformamide / 20 h / 20 °C 4: 77 percent / p-TsOH*H2O / methanol; dioxane / 1) 1 h, 60 deg C, 2) 45 min, 85 deg C View Scheme
参考文献
Nakano; Ito; Ogawa
Carbohydrate Research, 1993 , vol. 243, # 1 p. 43 - 69
反应条件
Yield given. Multistep reaction;
参考文献
Carbohydrate Research, , vol. 243, # 1 p. 43 - 69
