5-甲基-4-己烯-3-酮合成路线 （共 36 条）
反应条件
1: With [2-(methoxymethy)phenyl]phenylsilane; RhCl(PPh3)3 T=20°C; 2.5 h; 2: With hydrogenchloride
参考文献
Imao, Daisuke; Hayama, Miyuki; Ishikawa, Kohta; Ohta, Tetsuo; Ito, Yoshihiko
Chemistry Letters, 2007 , vol. 36, # 3 p. 366 - 367
反应条件
platinum Hydrogenation;
参考文献
Nasarow; Kuwarsina
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 1329
Chem.Abstr., 1949 , p. 2161
反应条件
ammonium hydroxide; trifluorormethanesulfonic acid 2 h; Heating;
参考文献
Bulletin de la Societe Chimique de France, , # 3 p. 454 - 458
反应条件
aluminium trichloride; ammonia 1.) 35 deg C, 1.5 h; Yield given. Multistep reaction. Further byproducts given;
参考文献
Erre, Claude H.; Roussel, Christian
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 11-12 p. 454 - 457
反应条件
1: ethyl bromide With magnesium in tetrahydrofuran
2: (2-methyl-1-propenyl)carbonyl chloride With anhydrous iron chloride in tetrahydrofuran; toluene
T=-40°C; 6 h; Cooling with acetone-dry ice;
3: With hydrogenchloride; water in tetrahydrofuran; toluene
参考文献
Takasago International Corporation
Patent: JP2005/170811 A, 2005 ;
Location in patent: Page/Page column 12 ;
反应条件
aluminium trichloride in chloroform
3 h;
参考文献
Heathcock, Clayton H.; Pirrung, Michael C.; Lampe, John; Buse, Charles T.; Young, Steven D.
Journal of Organic Chemistry, 1981 , vol. 46, # 11 p. 2290 - 2300
反应条件
formic acid; sodium formate
参考文献
Wilson,J.W.
Journal of the American Chemical Society, 1969 , vol. 91, # 12 p. 3238 - 3243
反应条件
ammonium hydroxide; methanesulfonic acid
T=85°C; Further byproducts given;
参考文献
Graindorge, Herve; Roussel, Christian
Bulletin de la Societe Chimique de France, 1986 , # 3 p. 454 - 458
反应条件
methanesulfonic acid
T=85°C; Further byproducts given;
参考文献
Graindorge, Herve; Roussel, Christian
Bulletin de la Societe Chimique de France, 1986 , # 3 p. 454 - 458
反应条件
copper; zinc in diethyl ether
参考文献
Dumont,C.; Vidal,M.
Bulletin de la Societe Chimique de France, 1973 , p. 2301 - 2312
