[苯甲酰基-[(4-氯苯基)甲氧基]氨基]乙酸酯合成路线 (共 13 条)
反应条件
in acetone Ambient temperature;
参考文献
Campbell, John J.; Glover, Stephen A.; Hammond, Gerard P.; Rowbottom, Colleen A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 12 p. 2067 - 2080
反应条件
1: 55 percent / potassium hydroxide, hydroxylamine hydrochloride / methanol 2: 95 percent / sodium carbonate / methanol; H2O / Heating 3: tert-butyl hypochlorite / CH2Cl2 / 5 h 4: 96 percent / acetone / Ambient temperature View Scheme
参考文献
Campbell, John J.; Glover, Stephen A.; Hammond, Gerard P.; Rowbottom, Colleen A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 12 p. 2067 - 2080
反应条件
1: tert-butyl hypochlorite / CH2Cl2 / 5 h 2: 96 percent / acetone / Ambient temperature View Scheme
参考文献
Campbell, John J.; Glover, Stephen A.; Hammond, Gerard P.; Rowbottom, Colleen A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 12 p. 2067 - 2080
反应条件
1: 95 percent / sodium carbonate / methanol; H2O / Heating 2: tert-butyl hypochlorite / CH2Cl2 / 5 h 3: 96 percent / acetone / Ambient temperature View Scheme
参考文献
Campbell, John J.; Glover, Stephen A.; Hammond, Gerard P.; Rowbottom, Colleen A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 12 p. 2067 - 2080
反应条件
1: 95 percent / sodium carbonate / methanol; H2O / Heating 2: tert-butyl hypochlorite / CH2Cl2 / 5 h 3: 96 percent / acetone / Ambient temperature View Scheme
参考文献
Campbell, John J.; Glover, Stephen A.; Hammond, Gerard P.; Rowbottom, Colleen A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 12 p. 2067 - 2080
反应条件
1: HBr-H2SO4 / diethyl ether / Heating 2: 95 percent / sodium carbonate / methanol; H2O / Heating 3: tert-butyl hypochlorite / CH2Cl2 / 5 h 4: 96 percent / acetone / Ambient temperature View Scheme
参考文献
Campbell, John J.; Glover, Stephen A.; Hammond, Gerard P.; Rowbottom, Colleen A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 12 p. 2067 - 2080
反应条件
1: toluene / 90 °C 2: hydroxylamine hydrochloride / pyridine; ethanol / Reflux View Scheme
参考文献
Johns, Jennifer P.; Van Losenoord, Arjan; Mary, Clement; Garcia, Pierre; Pankhurst, Damian S.; Rosser, Adam A.; Glover, Stephen A.
Australian Journal of Chemistry, 2010 , vol. 63, # 12 p. 1717 - 1729
反应条件
1: toluene / 90 °C 2: hydroxylamine hydrochloride / pyridine; ethanol / Reflux 3: deuterated toluene / 90 °C View Scheme
参考文献
Johns, Jennifer P.; Van Losenoord, Arjan; Mary, Clement; Garcia, Pierre; Pankhurst, Damian S.; Rosser, Adam A.; Glover, Stephen A.
Australian Journal of Chemistry, 2010 , vol. 63, # 12 p. 1717 - 1729
参考文献
Johns, Jennifer P.; Van Losenoord, Arjan; Mary, Clement; Garcia, Pierre; Pankhurst, Damian S.; Rosser, Adam A.; Glover, Stephen A.
Australian Journal of Chemistry, 2010 , vol. 63, # 12 p. 1717 - 1729
参考文献
Johns, Jennifer P.; Van Losenoord, Arjan; Mary, Clement; Garcia, Pierre; Pankhurst, Damian S.; Rosser, Adam A.; Glover, Stephen A.
Australian Journal of Chemistry, 2010 , vol. 63, # 12 p. 1717 - 1729