4-氯-2-三甲基甲硅烷基吡啶合成路线 （共 19 条）
反应条件
1: With copper(l) iodide; tetrabutyl ammonium fluoride in tetrahydrofuran; N,N-dimethyl-formamide T=20°C; 0.0833333 h; Inert atmosphere; 2: With oxygen in tetrahydrofuran; N,N-dimethyl-formamide T=20°C; 12 h;
参考文献
Louerat, Frederic; Gros, Philippe C.
Tetrahedron Letters, 2010 , vol. 51, # 27 p. 3558 - 3560
反应条件
copper(l) iodide; tetrabutyl ammonium fluoride; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran; N,N-dimethyl-formamide T=20°C; Hiyama cross-coupling; 12 h; Title compound not separated from byproducts;
参考文献
Pierrat, Philippe; Gros, Philippe; Fort, Yves
Organic Letters, 2005 , vol. 7, # 4 p. 697 - 700
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; triphenylphosphine in tetrahydrofuran; N,N-dimethyl-formamide T=20°C; 12 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 51, # 27 p. 3558 - 3560
反应条件
bis-triphenylphosphine-palladium(II) chloride; tetrabutyl ammonium fluoride; silver(l) oxide in N,N-dimethyl-formamide T=90°C; 3 h; Inert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 6 p. 1768 - 1773
反应条件
bis-triphenylphosphine-palladium(II) chloride; tetrabutyl ammonium fluoride; silver(l) oxide in N,N-dimethyl-formamide T=90°C; 3 h; Inert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 6 p. 1768 - 1773
反应条件
bis-triphenylphosphine-palladium(II) chloride; tetrabutyl ammonium fluoride; silver(l) oxide in N,N-dimethyl-formamide T=90°C; 3 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 6 p. 1768 - 1773
反应条件
tetrakis(triphenylphosphine) palladium(0); silver fluoride; silver(l) oxide in N,N-dimethyl-formamide T=90°C; Inert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 6 p. 1768 - 1773
反应条件
potassium fluoride; tetrakis(triphenylphosphine) palladium(0); silver(l) oxide in N,N-dimethyl-formamide T=90°C; Inert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 6 p. 1768 - 1773
反应条件
bis-triphenylphosphine-palladium(II) chloride; tetrabutyl ammonium fluoride; silver(l) oxide in N,N-dimethyl-formamide
T=90°C; 3 h; Inert atmosphere;
参考文献
Louerat, Frederic; Tye, Heather; Napier, Spencer; Garrigou, Michael; Whittaker, Mark; Gros, Philippe C.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 6 p. 1768 - 1773
