反应条件
ammonium sulfate in dichloromethane
under nitrogen: PCl5, ammonium sulfate refluxed in dichloromethane for one h under stirring, cooled to room temp.; filtered, evapn. under reduced pressure;
参考文献
Delpuech, J. J.; Fasan, G.; Rodehueser, L.; Rubini, P.; Selve, C.
Phosphorus and Sulfur and the Related Elements, 1988 , vol. 35, p. 281 - 290