4,4-二甲基-1-苯戊烷-1,3-二酮合成路线 （共 34 条）
反应条件
sodium hydride 1.) THF, reflux, 30 min, 2.) THF, reflux 2 h; Yield given. Multistep reaction;
参考文献
Australian Journal of Chemistry, , vol. 45, # 5 p. 865 - 875
参考文献
Chemistry - A European Journal, , vol. 9, # 18 p. 4485 - 4509
反应条件
T=200°C; P=73550.8 Torr;
参考文献
Beckham; Adkins
Journal of the American Chemical Society, 1934 , vol. 56, p. 2676,2678
参考文献
Vorlaender; Kalkow
Chemische Berichte, 1897 , vol. 30, p. 2271
参考文献
Vorlaender; Kalkow
Chemische Berichte, 1897 , vol. 30, p. 2271
反应条件
N-ethyl-N,N-diisopropylamine; magnesium bromide in dichloromethane
4 h;
参考文献
Lim, Daniel; Zhou, Guoqiang; Livanos, Alexandra E.; Fang, Fang; Coltart, Don M.
Synthesis, 2008 , # 13 p. 2148 - 2152
反应条件
N-ethyl-N,N-diisopropylamine; magnesium bromide in dichloromethane
24 h;
参考文献
Lim, Daniel; Zhou, Guoqiang; Livanos, Alexandra E.; Fang, Fang; Coltart, Don M.
Synthesis, 2008 , # 13 p. 2148 - 2152
反应条件
sodium hydride in toluene
RefluxInert atmosphere;
参考文献
Russo, Alessio; Galdi, Gerardina; Croce, Gianluca; Lattanzi, Alessandra
Chemistry - A European Journal, 2012 , vol. 18, # 20 p. 6152 - 6157
反应条件
samarium diiodide in tetrahydrofuran
T=20°C; Reformatsky type reaction; 1 h;
参考文献
Baek, Heung Soo; Yoo, Byung Woo; Keum, Sam Rok; Yoon, Cheol Min; Kim, Sung Hoon; Kim, Joong Hyup
Synthetic Communications, 2000 , vol. 30, # 1 p. 31 - 38
反应条件
gallium triiodide in acetonitrile
T=20°C; Acylation; 1 h;
参考文献
Chen, Rener; Wu, Huayue; Zhang, Yongmin
Journal of Chemical Research - Part S, 1999 , # 11 p. 666 - 667
