4,4-二甲基-1-苯戊烷-1,3-二酮合成路线 （共 34 条）
反应条件
fluorine in acetonitrile
T=5 - 10°C; Continuous flow reactor apparatusInert atmosphere;
参考文献
Breen, Jessica R.; Sandford, Graham; Yufit, Dmitrii S.; Howard, Judith A. K.; Fray, Jonathan; Bhairavi, Patel
Beilstein Journal of Organic Chemistry, 2011 , vol. 7, art. no. 120, p. 1048 - 1054
反应条件
sodium tetrahydroborate; bovine serum albumin in water; acetonitrile
Title compound not separated from byproducts.;
参考文献
Benedetti, Fabio; Berti, Federico; Donati, Ivan; Fregonese, Massimo
Chemical Communications, 2002 , # 8 p. 828 - 829
反应条件
1: diiodomethane With diethylzinc; trifluoroacetic acid in dichloromethane
T=0°C; 0.5 h;
2: 4,4-dimethyl-1-phenylpentane-1,3-dione in dichloromethane
T=20°C; 5 h;
参考文献
Xue, Song; Li, Le-Zhen; Liu, Yong-Kang; Guo, Qing-Xiang
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 215 - 218
参考文献
Vorlaender; Kalkow
Chemische Berichte, 1897 , vol. 30, p. 2271
