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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
14001-37-7
合成路线
（共 8 条）
14001-37-7
+
68-12-2
N,N-二甲基甲酰胺
→
反应条件
21172-88-3
2-氯-5,6,7,8-四氢喹啉
反应条件
trichlorophosphate 1.) 2 h, room temperature, 2.) 75 deg C, 4 h;
参考文献
Meth-Cohn, Otto; Westwood, Keith T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 6 p. 1173 - 1182
14001-37-7
→
反应条件
28712-62-1
5,6,7,8-四氢-3-甲基喹啉
反应条件
1: 69 percent / POCl3 / CH2Cl2 / 3 h / 0 - 15 °C 2: 52 percent / POCl3 / 1,2-dichloro-ethane / 4 h / Heating View Scheme
参考文献
Boruah, Romesh C.; Ahmed, Shahadat; Sharma, Utpal; Sandhu, Jagir S.
Journal of Organic Chemistry, 2000 , vol. 65, # 3 p. 922 - 925
141-32-2
丙烯酸丁酯
+
14001-37-7
→
反应条件
59-31-4
2-羟基喹啉
反应条件
1: N-acetyl-3,4,5,6-tetrahydroaniline With tertiary butyl peroxybenzenoate; methylethyl sulfide; palladium diacetate in ethylene glycol dimethyl ether T=100°C; 2: acrylic acid n-butyl ester With toluene-4-sulfonic acid in ethylene glycol dimethyl ether; water T=80°C; 2 h; 3: With hydrogenchloride in ethylene glycol dimethyl ether; water T=80°C; 16 h;
参考文献
Kim, Jinhee; Moon, Youngtaek; Lee, Suhyun; Hong, Sungwoo
Chemical Communications, 2014 , vol. 50, # 24 p. 3227 - 3230
14001-37-7
→
反应条件
765-87-7
1,2-环己二酮
反应条件
1: SeO2 / dioxane 2: aq. HCl / ethanol View Scheme
参考文献
Boar,R.B. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 1237 - 1241
14001-37-7
→
反应条件
1658-08-8
1,2,3,4,5,6,7,8-八氢吖啶
反应条件
1: 69 percent / POCl3 / CH2Cl2 / 3 h / 0 - 15 °C 2: 51 percent / POCl3 / 1,2-dichloro-ethane / 4 h / Heating View Scheme
参考文献
Boruah, Romesh C.; Ahmed, Shahadat; Sharma, Utpal; Sandhu, Jagir S.
Journal of Organic Chemistry, 2000 , vol. 65, # 3 p. 922 - 925
591-50-4
碘苯
+
14001-37-7
→
反应条件
2113-47-5
N-(2-苯基苯基)乙酰胺
反应条件
1: N-acetyl-3,4,5,6-tetrahydroaniline With methylethyl sulfide; silver(I) acetate; palladium diacetate in ethylene glycol dimethyl ether T=100°C; 3.5 h; 2: iodobenzene With copper(II) bis(trifluoromethanesulfonate) in ethylene glycol dimethyl ether T=100°C;
参考文献
Kim, Jinhee; Moon, Youngtaek; Lee, Suhyun; Hong, Sungwoo
Chemical Communications, 2014 , vol. 50, # 24 p. 3227 - 3230
141-32-2
丙烯酸丁酯
+
14001-37-7
→
反应条件
59-31-4
2-羟基喹啉
反应条件
1: N-acetyl-3,4,5,6-tetrahydroaniline With tertiary butyl peroxybenzenoate; methylethyl sulfide; palladium diacetate in ethylene glycol dimethyl ether T=100°C; 2: acrylic acid n-butyl ester With toluene-4-sulfonic acid in ethylene glycol dimethyl ether; water T=80°C; 2 h; 3: With hydrogenchloride in ethylene glycol dimethyl ether; water T=80°C; 16 h;
参考文献
Kim, Jinhee; Moon, Youngtaek; Lee, Suhyun; Hong, Sungwoo
Chemical Communications, 2014 , vol. 50, # 24 p. 3227 - 3230
14001-37-7
→
反应条件
5908-28-1
反应条件
selenium(IV) oxide in 1,4-dioxane
参考文献
Boar,R.B. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 1237 - 1241
