反应条件
1: 98 percent / diethyl azodicarboxylate; Ph3P / tetrahydrofuran; toluene / 2 h / Heating
2: 97 percent / LiAlH4 / tetrahydrofuran / 1.5 h / 0 °C
3: 89 percent / PDC; 4 Angstroem molecular sieves / CH2Cl2 / 20 °C
4: 3.82 g / diethyl ether / 1.5 h / -78 °C
5: 81 percent / 2,6-lutidine / CH2Cl2 / 0.08 h / 0 °C
6: 77 percent / aq. CAN / acetonitrile / 0.25 h / 0 °C
View Scheme
参考文献
Fujishima, Toshie; Kittaka, Atsushi; Yamaoka, Kazuyoshi; Takeyama, Ken-Ichi; Kato, Shigeaki; Takayama, Hiroaki
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 11 p. 1863 - 1869
