1-(3,4-二氢-2(1H)-异喹啉基)乙酮合成路线 (共 29 条)
反应条件
potassium iodide in 1,2-dichloro-ethane 2 h; Ambient temperature;
参考文献
Venkov; Lukanov
Synthesis, 1989 , # 1 p. 59 - 61
反应条件
sodium iodide in acetonitrile T=60°C; 40 h;
参考文献
Ihara, Masataka; Hirabayashi, Akihito; Taniguchi, Nobuaki; Fukumoto, Keiichiro
Heterocycles, 1992 , vol. 33, # 2 p. 851 - 858
反应条件
sodium tetrahydroborate in acetic acid T=60°C; 2 h; Product distribution;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 28, # 7 p. 2226 - 2228
反应条件
methyl (triphenylphosphoranylidene)acetate in dichloromethane 120 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 37, # 8 p. 1233 - 1236
反应条件
1: Na2SO4 / 1,2-dichloro-ethane / 0.5 h / Heating 2: 1.) SOCl2, KI / 1.) 1,2-dichloroethane, room temp., 1 h, 2.) room temp., 3 h View Scheme
参考文献
Synthesis, , # 1 p. 59 - 61
反应条件
in methanol; dichloromethane 120 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 37, # 8 p. 1233 - 1236
反应条件
thionyl chloride; potassium iodide 1.) 1,2-dichloroethane, room temp., 1 h, 2.) room temp., 3 h; Yield given. Multistep reaction;
参考文献
Synthesis, , # 1 p. 59 - 61
反应条件
ethylmagnesium bromide 1.) THF, 70 deg C, 15 min, 2.) THF, 70 deg C, 2 min; Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 19 p. 2837 - 2842
参考文献
Chemische Berichte, , vol. 26, p. 1211
反应条件
2-hydroxy-1,3-isoindolinedione; oxygen; anhydrous cobalt diacetate; metachloroperbenzoic acid in acetonitrile T=20°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 67, # 8 p. 2671 - 2676